Selective suppression and excitation of solid-state NMR resonances based on quadrupole coupling constants

Journal of Magnetic Resonance

Volumn 160, Issue 2, 2003, Pages 107-113

  Kwak, Hyung Tae ^a   Prasad, Subramanian ^a   Clark, Ted ^a   Grandinetti, Philip J ^a  

^a OHIO STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

MAGNETIZATION; POLARIZATION; RUBIDIUM COMPOUNDS; SPECTRUM ANALYSIS;

QUADRUPOLE COUPLING;

NUCLEAR MAGNETIC RESONANCE;

EID: 0042415778     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1090-7807(02)00139-8     Document Type: Article

References (19)

1. Caldarelli S., Ziarelli F. Spectral editing of solid-state MAS NMR spectra of half-integer quadrupolar nuclei. J. Am. Chem. Soc. 122:2000;12015-12016.
2. Skibsted J., Nielsen N.C., Bildsoe H., Jakobsen H.J. Satellite transitions in MAS NMR spectra of quadrupolar nuclei. J. Magn. Reson. 95:1991;88-117.
3. Haase J., Curro N.J., Stern R., Slichter C.P. New methods for NMR of cuprate superconductors. Phys. Rev. Lett. 81:1998;1489-1492.
4. Yao Z., Kwak H.-T., Sakellariou D., Emsley L., Grandinetti P.J. Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning. Chem. Phys. Lett. 327:2000;85-90.
5. Kwak H.-T., Prasad S., Yao Z., Grandinetti P.J., Sachleben J.R., Emlsey L. Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer. J. Magn. Reson. 150:2001;71-80.
6. Prasad S., Kwak H.T., Clark T., Grandinetti P.J. A simple technique for determining nuclear quadrupole coupling constants using RAPT solid-state NMR spectroscopy. J. Am. Chem. Soc. 124(18):2002;4964-4965.
7. Pound R.V. Nuclear electric quadrupole interactions in crystals. Phys. Rev. 79:1950;685-702.
8. Vega S., Naor Y. Triple quantum NMR on spin systems with. I=3/2 in solids J. Chem. Phys. 75:1981;75.
9. Haase J., Conradi M.S. Sensitivity enhancement for NMR of the central transition of quadrupolar nuclei. Chem. Phys. Lett. 209(3):1993;287-291.
10. Haase J., Conradi M.S., Oldfield E. Single- and double-resonance experiments of quadrupolar nuclei in solids using sensitivity enhancement of the central transition. J. Magn. Reson. A. 109:1994;210-215.
11. Haase J., Conradi M.S., Grey C.P., Vega A.J. Population transfers for NMR of quadrupolar spins in solids. J. Magn. Reson. A. 109:1994;90-97.
12. Kentgens A.P.M., Verhagen R. Advantages of double frequency sweeps in static, MAS, and MQMAS NMR of spin. I=3/2 nuclei Chem. Phys. Lett. 300:1999;435-443.
13. 4 J. Magn. Reson. 122:1996;111-119.
14. Grandinetti P.J., Baltisberger J.H., Llor A., Lee Y.K., Werner U., Eastman M.A., Pines A. Pure absorption-mode lineshapes and sensitivity in two-dimensional dyanmic angle spinning NMR. J. Magn. Reson. A. 103:1993;72-81.
15. Wu G., Rovnyak D., Griffin R.G. Quantitative multiple-quantum magic-angle spinning NMR spectroscopy of quadrupolar nuclei in solids. J. Am. Chem. Soc. 118:1996;9326-9332.
16. Massiot D. Sensitivity and lineshape improvements of MQ-MAS by rotor-synchronized data acquisition. J. Magn. Reson. A. 122:1996;240.
17. Hodgkinson P., Emsley L. Numerical simulation of solid-state NMR experiments. Prog. Nucl. Magn. Reson. Spectrosc. 36(3):2000;201-239.
18. Lim K.H., Charpentier T., Pines A. Efficient triple-quantum excitation in modified RIACT MQMAS NMR for. I=3/2 nuclei J. Magn. Reson. 154:2002;196-204.
19. Madhu P.K., Levitt M.H. Signal enhancement in the triple-quantum magic-angle spinning NMR of spins-3/2 in solids: The FAM-RIACT-FAM sequence. J. Magn. Reson. 155:2002;150-155.