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Although it affords less in terms of the yield, Z protection of the amino group in TRIS by this method was very straightforward, and the product was obtained in high purity. For another method of preparation, see ref. [23 d].
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84891321103
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Polygen Corporation, 200 Fifth Avenue, Waltham, MA 02254, USA
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Polygen Corporation, 200 Fifth Avenue, Waltham, MA 02254, USA.
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85
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84891342360
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note
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2O = acetic anhydride; app. = apparent; BOC = tert-butyloxycarbonyl; Bz = benzoyl; DCC = 1,3-dicyclohexylcarbodiimide; Glc = glucose; Gly = glycine; HOBT =1-hydroxybenzotriazole; PFP = pentafluorophenyl; TRIS = tris(hydroxymethyl)methylamine; Z = benzyloxycarbonyl.
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