Development of a method for the measurement of dehydroepiandrosterone sulphate by liquid chromatography-tandem mass spectrometry

Annals of Clinical Biochemistry

Volumn 42, Issue 6, 2005, Pages 468-474

  Chadwick, Carrie A ^a   Owen, L J ^a   Keevil, B G ^a  

^a WYTHENSHAWE HOSPITAL   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

PRASTERONE SULFATE;

ACCURACY; ANALYTIC METHOD; ARTICLE; HUMAN; LINEAR SCLERODERMA; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; QUALITY CONTROL; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY; TIME;

CHROMATOGRAPHY, LIQUID; DEHYDROEPIANDROSTERONE SULFATE; DOSE-RESPONSE RELATIONSHIP, DRUG; HUMANS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 27844585182     PISSN: 00045632     EISSN: 00045632     Source Type: Journal    
DOI: 10.1258/000456305774538175     Document Type: Article

References (18)

1. Leowattana W. DHEAS as a new diagnostic tool. Clin Chim Acta 2004; 341: 1-15
2. Longcope C. Dehydroepiandrosterone metabolism. J Endocrinol 1996; 150: S125-7
3. Bird CE, Masters V, Clark AF. Dehydroepiandrosterone sulfhate: kinetics of metabolism in normal young men and women. Clin Invest Med 1984; 7: 119-22
4. Chang PL, Lindheim SR, Lowre C, et al. Normal ovulatory women with polycystic ovaries have hyperandrogenic pituitary-ovarian responses to gonadotrophin releasing hormone agonist testing. J Clin Endocrinol Metab 2000; 85: 995-1000
5. Lewis JG, Bason LM, Elder PA. Production and characterization of monoclonal antibodies to dehydroepiandrosterone sulfate: application to direct enzyme-linked immunosorbent assays of dehydroepiandrosterone sulfate and androsterone/epiandrosterone sulfates in plasma. Steroids 1996; 61: 682-7
6. Elmlinger MW, Dengler T, Weinstock C, Kuhnel W. Endocrine alterations in the aging male. Clin Chem Lab Med 2003; 41: 934-41
7. Elmlinger MW, Kuhnel W, Ranke MB. Reference ranges for serum concentrations of lutropin (LH), follitropin (FSH), estradiol (E2), prolactin, progesterone, sex hormone-binding globulin (SHBG), dehydroepiandrosterone sulfate (DHEAS), cortisol and ferritin in neonates, children and young adults. Clin Chem Lab Med 2002; 40: 1151-60
8. Remer T, Pietrzik K, Manz F. Measurement of urinary androgen sulfates without previous hydrolysis: a tool to investigate adrenarche. Validation of a commercial radioimmunoassay for dehydroepiandrosterone sulfate. Steroids 1994; 59: 10-5
9. Dhar TK, Muller C, Schoneshofer M. Determination of dehydroepiandrosterone sulfate in plasma by a one-step enzyme immunoassay with a microtitre plate. Clin Chem 1985; 31: 1876-9
10. Serizawa S, Nagai T, Ito M, Sato Y. Simplified determination of serum cholesterol sulfate by gas-liquid chromatography combined with cyclohexylsilane-bonded phase column purification. Arch Dermatol Res 1989; 281: 411-6
11. Zemaitis MA, Kroboth PD. Simplified procedure for measurement of serum dehydroepiandrosterone and its sulfate with gas chromatography-ion trap mass spectrometry and selected reaction monitoring. J Chromatogr B Biomed Sci Appl 1998; 716: 19-26
12. Nakajima M, Yamato S, Shimada K. Determination of dehydroepiandrosterone sulphate in biological samples by liquid chromatography/atmospheric pressure chemical ionisation-mass spectrometry using [7, 7, 16, 16-2H4]- dehydroepiandrosterone sulphate as an internal standard. Biomed Chromatogr 1998; 12: 211-6
13. 2 monitoring. Ther Drug Monit 2002; 24: 757-67
14. Keevil BG, McCann SJ, Cooper DP, Morris MR. Evaluation of a rapid micro-scale assay for tacrolimus by liquid chromatography-tandem mass spectrometry. Ann Clin Biochem 2002; 39: 487-92
15. Keevil BG, Newman S, Lockhart S, Howard SJ, Moore CB, Denning DW. Validation of an assay for voriconazole in serum samples using liquid chromatography-tandem mass spectrometry. Ther Drug Monit 2004; 26: 650-7
16. Owen LJ, Gillingwater S, Keevil BG. Prednisolone measurement in human serum using liquid chromatography tandem mass spectrometry. Ann Clin Biochem 2005; 42: 105-11
17. McCann SJ, Gillingwater S, Keevil BG. Measurement of urinary free cortisol using liquid chromatography-tandem mass spectrometry: comparison with the urine adapted ACS:180 serum cortisol chemiluminescent immunoassay and development of a new reference range. Ann Clin Biochem 2005; 42: 112-8
18. Corporate author. US department of Health and Human Services Food and Drug Administration, Center for Drug Evaluation and Research (CDER), Center for Veterinary Medicine (CVM). Guidance For Industry Bioanalytical Method Validation; May 2001: 1-22