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85030743342
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note
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The complexation induced shift of the guest proton is less than 0.01 ppm in the presence of 5 equiv excess of 3.
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o|. The structures were solved by the direct method (SHELXL-97). Full-matrix least squares refinements converged to a conventional R factor of 0.096, wR = 0.237 (I > 2σ(I)). The crystallographic results have been deposited with the Cambridge Crystallographic Data Centre, UK as supplementary publication number CCDC No. 245021. Copy of the data can be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033 or e-mail: data_request@ccdc.cam. ac.uk.
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25
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85030748167
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note
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o|. The structures were solved by the direct method (SHELXL-97). Full-matrix least squares refinements converged to a conventional R factor of 0.122, wR = 0.289 (I > 2σ(I)). The crystallographic results have been deposited with the Cambridge Crystallographic Data Centre, UK as supplementary publication number CCDC No. 245022.
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