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27744555289
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note
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21 + 1: 387.9937, Found: 387.9951.
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-
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21
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27744515123
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note
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19: 390.0345, Found: 390.0293.
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22
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27744579136
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note
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5: 336.0126, Found: 336.0136.
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27744466948
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note
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-1 of wire burned has been applied in all standardization and calorific value determinations. Acid correction has been omitted for all semimicro samples. The bomb was examined for evidence of unburned compound after each run, and, if more than a slight trace was present, the run was discarded.
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31
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37049094806
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32
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27744477186
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note
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a (N-H). NMR: 1H, δ 1.41 [s, 9H (t-Bu)], 3.16 [d (J = 3 Hz) N-H]; 13C, δ 31.1 (d, J = 6 Hz); 31P{1H}, δ -2.3 (t, J = 43 Hz), -6.8 (t, J = 43).
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-
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33
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27744474630
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note
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2 = 0.1134 for [I > 2σ(I)]. CCDC 278747. See http://dx.doi.org/10.1039/b510924h for crystallographic data in CIF or other electronic format. The t-Bu group was disordered and modeled in two positions with occupancies of 0.74 and 0.16. Loose restraints were applied to keep C-C distances reasonable.
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34
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0000303704
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