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-1, reflections measured 32 846, 8249 unique reflections, 5709 observed reflections [I > 2σ (I)], R1_obs = 0.055, wR2_obs = 0.126.
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11
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0001835759
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77 of the 82 compounds in the Cambridge Structural Database (CSD, Feb 2005 update, Screens: R ≤ 7.5, 3D coordinates determined, only organics; Allen, F. H.; Kennard, O. Chem. Des. Automat. News 1993, 8, 31) that contain carboxylic acid and pyridyl groups in the absence of competing groups form supramolecular heterosynthon I.
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Allen, F.H.1
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2242428043
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Imidazoles and carboxylic acids form related supramolecular synthons: MacDonald, J. C.; Dorrestein, P. C.; Pilley, M. M. Cryst. Growth Des. 2001, 1, 29.
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24
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27744587384
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note
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-1, 11 890 reflections measured, 4096 unique reflections, 2152 observed reflections [I > 2σ(I)], R1_obs = 0.062, wR2_obs = 0.124.
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26
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0002464446
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