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note
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Thermal stabilities were determined by immersion of the vial upside down in a thermocontrolled bath.
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17
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27644533395
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note
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The NMR tube was shaken after addition of the amine to avoid diffusion limitations. It is well-known that diffusion processes are slow in the gel medium and that the shape of the container also plays an important role in the strength of the gel. When samples were not shaken, a slow diffusion of the amine could be detected.
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18
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