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IIb accommodated one TTF molecule to give 2⊃DTTF, which showed a similar CT band around 680 nm. Neither cyclic voltainmogram nor electric absorption spectrum of 2DTTF showed any peaks for mixed-valence species,
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0041817633
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25844516760
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note
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(a) The fluid behavior of relatively small TTF molecules in the cavity of 1 (on the NMR time scale) may be another cause for broadening of the proton signal,
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21
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note
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2 was estimated to be >88%). Probably, TTF was partially lost during isolation procedures. See the Supporting Information.
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