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0036277343
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9
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0028819889
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10
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0032078243
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14
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25444481263
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note
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The detailed preparation and characterization of 10 and 11 is provided in the Supporting Information.
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15
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0035932575
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Kataoka, M.; Hattori, A.; Okino, S.; Hyodo, M.; Asano, M.; Kawai, R.; Hayakawa, Y. Org. Lett. 2001, 3, 815-818.
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Kawai, R.6
Hayakawa, Y.7
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16
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25444467406
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note
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The use of ethy(methyl)dioxirane as an oxidant over iodine or tert-butyl hydroperoxide produced 17a-d in higher yields.
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-
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17
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0025161168
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(a) Iyer, R. P.; Phillips, L. R.; Egan, W.; Regan, J. B.; Beaucage, S. L. J. Org. Chem. 1990, 55, 4693-4699.
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18
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0000839769
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Phillips, L.R.2
Org, B.S.L.3
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19
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25444508168
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note
-
Experimental parameters and conditions for the automated synthesis of 5′-phosphorylated oligonucleotides are provided in the Supporting Information.
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-
-
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20
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25444523945
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note
-
RP-HPLC profiles of crude and deprotected oligonucleotides are shown in the Supporting Information along with the MALDI-TOF mass spectral analysis of each oligonucleotide.
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21
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0343959655
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Marugg, J. E.; Burik, A.; Tromp, M.; van der Marel, G. A.; van Boom, J. H. Tetrahedron Lett. 1986, 27, 2271-2274.
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Van Boom, J.H.5
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23
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25444435343
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note
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31P NMR data.
-
-
-
-
24
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25444523429
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note
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31P NMR spectroscopy.
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