Crystal structure of 2-(6-[2-(5-ethyl-5-hydroxy-6-methyl-tetrahydro-pyran2- yl)-15-oxo-2,10,12-trimethyl-1,6,8-trioxa-dispiro[4.1.5.3]pentadec-13-en-9-yl] -2-hydroxy-1,3-dimethyl-4-oxo-heptyl-5-methyl-tetrahydro-pyran-2-yl)-butyrate sodium, Na(C42H67O11), SY-9 - Antibiotic 20-oxo-salinomycin

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 219, Issue 2, 2004, Pages 184-186

  Paulus, E F ^a   Vertesy L ^b  

^a GOETHE UNIVERSITY   (Germany)

^b SANOFI AVENTIS DEUTSCHLAND GMBH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 24944507718     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: 10.1524/ncrs.2004.219.2.184     Document Type: Article

References (12)

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2. Flack, H. D.; Bernardinelli, G.: Absolute structure and absolute configuration. Acta Crystallogr. A55 (1999) 908-915.
3. Hamilton, W. C.: Significance Tests on the Crystallographic R Factors. Acta Crystallogr. 18 (1965) 502-510.
4. Miyazaki, Y.; Shibuya, M.; Sugawara, H.; Kawaguchi, O.; Hirsoe, C.: Salinomycin, a newpolyetherantibiotic. J. Antibiotics 27 (1974) 814-821.
5. Miyazaki, Y.; Shibata, A.; Tsuda, K.; Kinashi, H.; Otake, N.: Studies on the ionophorous antibiotics. Isolation, characterisation and structure of SY-1. Agric. Biol. Chem. 42 (1978) 2129-2132.
6. Kinashi, H.; Otake, N.; Yonehara, H.; Sato, S.; Saito, Y.: Studies on the Ionophorous Antibiotics. I. The Crystal and Molecular Structure of Salinomycin p-Iodophenacyl Ester. Acta Crystallogr. B31 (1975) 2411-2415.
7. Paulus, E. F.; Kurz, M.; Matter, H.; Vértesy, L.: Solid-State and Solution Structure of the Salinomycin-Sodium Complex: Stabilization of Different Conformers for an Ionophore in Different Environments. J. Am. Chem. Soc. 120 (1998) 8209-8221.
8. Paulus, E. F.; Vértesy, L.: The Antibiotic Salinomycin and another three Derivatives. Lecture MS2.6-6, 17th European Crystallographic Meeting, Lisboa 1997; Poster, Computing School on Practical Aspects of Charge Density Determination, Berlin 1997.
9. 3OH. Z. Kristallogr. NCS 218 (2003) 575-577.
10. Sheldrick, G. M.: SHELXS-97. Program for the Solution of Crystal Structures. University of Göttingen, Germany 1997.
11. Sheldrick, G. M.: SHELXL-97. Program for the Refinement of Crystal Structures. University of Göttingen, Germany 1997.
12. Sheldrick, G. M.: SHELXTL-PLUS, Release 5.10. An Integrated System for Solving, Refining and Displaying Crystal Structures from Diffraction Data. Bruker Analytical Systems, Madison, Wisconsin USA 1997.