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(b) Isothermal titration calorimetery (ITC) measurements were performed as follows. Solutions of the chosen receptor in rigorously dry acetonitrile were made up so as to provide a receptor concentration range of 0.1-1 mM. These solutions were then individually titrated with the appropriate alkylammonium salts at 30 ± 0.01 °C. The original heat pulses were normalized using reference titrations carried out using the same salt solution but pure solvent, as opposed to a solution containing the receptor.
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