First synthesis of a selenazepane

Tetrahedron Letters

Volumn 46, Issue 39, 2005, Pages 6723-6725

  Sommen, Geoffroy L ^a   Linden, Anthony ^a   Heimgartner, Heinz ^a  

^a UNIVERSITY OF ZURICH   (Switzerland)

Author keywords

Isoselenocyanate; Selenazepane; Selenium

Indexed keywords

AMINE; ISOCYANIC ACID DERIVATIVE; SELENAZEPANE; SELENIUM DERIVATIVE; TRIETHYLAMINE; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; DRUG STRUCTURE; DRUG SYNTHESIS; EVAPORATION; STRUCTURE ANALYSIS;

EID: 23944431849     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.07.127     Document Type: Article

References (37)

1. T. Wirth Tetrahedron 55 1999 1 28
2. V.P. Litvinov, and V.D. Dyachenko Russ. Chem. Rev. 66 1997 923 951
3. T. Wirth Organoselenium Chemistry Topics in Current Chemistry Vol. 208 2000 Springer Berlin
4. T.G. Back Organoselenium Chemistry, A Practical Approach 1999 Oxford Oxford University Press
5. A. Wengel Selenium in Biology and Medicine 1989 Springer Berlin
6. R.F. Burk Selenium in Biology and Human Health 1994 Springer New York
7. Y. Xu, and E.T. Kool J. Am. Chem. Soc. 122 2000 9040 9041
8. H.E. Ganther Bioorg. Med. Chem. 9 2001 1459 1466
9. G. Mugesh, W.-W. Du Mont, and H. Sies Chem. Rev. 101 2001 2125 2180
10. S.W. May Exp. Opin. Invest. Drugs 11 2002 1261 1269
11. R.J. Shamberger Biochemistry of Selenium 1983 Plenum Press New York
12. D.L. Hatfield Selenium. Its Molecular Biology and Role in Human Health 2001 Kluwer Academic Boston
13. M.L. Petrov, and N.I. Zmitrovich Russ. J. Gen. Chem. 69 1999 245 256
14. D.H.R. Barton, S.I. Parekh, M. Tajbakhsh, E.A. Theodorakis, and C.-L. Tse Tetrahedron 50 1994 639 654
15. M.T. Bakhsh, Y.S. Behshtiha, and M.M. Heravi J. Chem. Soc. Pak. 18 1996 159 162
16. Y. Zhou, A. Linden, and H. Heimgartner Helv. Chim. Acta 83 2000 1576 1598
17. P.K. Atanassov, A. Linden, and H. Heimgartner Heterocycles 61 2003 569 579 and 2004, 62, 521-533
18. P.K. Atanassov, A. Linden, and H. Heimgartner Helv. Chim. Acta 87 2004 1452 1466 and 1873-1887
19. G.L. Sommen, A. Linden, and H. Heimgartner Helv. Chim. Acta 88 2005 766 773
20. G.L. Sommen, A. Linden, and H. Heimgartner Eur. J. Org. Chem. 14 2005 3127 3128
21. G.L. Sommen, A. Linden, and H. Heimgartner Heterocycles 65 2005 1903 1915
22. Sommen, G. L.; Linden, A.; Heimgartner, H. in preparation.
23. K.I. Nurbaev, K.A. Zakhidov, E.O. Oripov, R.A. Smiev, and K.M. Shakhidoyatov Uzb. Khim. Zh. 1-2 1996 96 101
24. Chem. Abstr. 126 1996 47303
25. P.L. Minin, and J.C. Walton J. Org. Chem. 68 2003 2960 2963
26. S. Ishikawa, N. Saitoh, and M. Mochizuki Chem. Pharm. Bull. 48 2000 1500 1503
27. +).
28. 2SeBrCl (367.92): C 35.85, H 3.83, N 7.60. Found: C 35.78, H 3.98, N 7.60.
29. -3.
30. CCDC-274506 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from the Cambridge Crystallographic Data Centre, via www.ccdc.cam.ac.uk/data_request/cif.
31. Hooft, R. KappaCCD Collect Software, Nonius BV, Delft, The Netherlands, 1999.
32. Z. Otwinowski, and W. Minor C.W. Carter Jr. R.M. Sweet Macromolecular Crystallography, Part A Methods in Enzymology Vol. 276 1997 Academic Press New York 307 326
33. R.H. Blessing Acta Crystallogr., Sect. A 51 1995 33 38
34. A. Altomare, G. Cascarano, C. Giacovazzo, A. Guagliardi, M.C. Burla, G. Polidori, and M. Camalli J. Appl. Crystallogr. 27 1994 435
35. G.M. Sheldrick shelxl97, Program for the Refinement of Crystal Structures 1997 Germany University of Göttingen
36. Johnson, C. K., ORTEP II, Report ORNL-5138; Oak Ridge National Laboratory: Oak Ridge, Tennessee, 1976.
37. J. Bernstein, R.E. Davis, L. Shimoni, and N.-L. Chang Angew. Chem., Int. Ed. Engl. 34 1995 1555 1573