Sterically congested in-methylcyclophanes

Journal of the American Chemical Society

Volumn 127, Issue 32, 2005, Pages 11246-11247

  Song, Qiuling ^a   Ho, Douglas M ^a   Pascal Jr , Robert A ^a  

^a PRINCETON UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CYCLOPHANE DERIVATIVE;

AB INITIO CALCULATION; ARTICLE; BROMINATION; CHROMATOGRAPHY; CRYSTALLIZATION; ISOMER; ISOMERISM; NUCLEAR MAGNETIC RESONANCE; POLYMERIZATION; SPECTROSCOPY; STEREOCHEMISTRY;

EID: 23844558770     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja0529384     Document Type: Article

References (27)

1. Review: Pascal, R. A., Jr. Eur. J. Org. Chem. 2004, 3763-3771.
2. Review: Alder, R. W.; East, S. P. Chem. Rev. 1996, 96, 2097-2111.
3. (a) Pascal, R. A., Jr.; Grossman. R. B. J. Org. Chem. 1987, 52, 4616-4617.
4. (b) Pascal, R. A., Jr.; Grossman, R. B.; Van Engen, D. J. Am. Chem. Soc. 1987, 109, 6878-6880.
5. (c) Pascal, R. A., Jr.; Winans, C. G.; Van Engen. D. J. Am. Chem. Soc. 1989, 111, 3007-3010.
6. Ilioudis, C. A.; Bearpark, M. J.; Steed, J. W. New J. Chem. 2005, 29, 64-67.
7. Kim, T. H.; Yang, S. Y.; Lee, S. S.; Kim, J. S.; Kim, J. Acta Crystallogr., Sect E 2001, 57, o1200-o1202.
8. L'Espérance, R. P.; West, A. P., Jr.; Van Engen, D.; Pascal, R. A., Jr. J. Am. Chem. Soc. 1991, 113, 2672-2676.
9. (a) Pascal, R. A., Jr.; West, A. P., Jr.; Van Engen, D. J. Am. Chem. Soc. 1990, 112, 6406-6407.
10. (b) West, A. P., Jr.; Smyth, N.; Kraml, C. M.; Ho, D. M.; Pascal, R. A., Jr. J. Org. Chem. 1993, 58, 3502-3506.
11. (c) Dell, S.; Ho, D. M.; Pascal, R. A., Jr. J. Org. Chem. 1999, 64, 5626-5633.
12. (d) Chen, Y. T.; Baldridge, K. K.; Ho, D. M.; Pascal, R. A., Jr. J. Am. Chem. Soc. 1999, 121, 12082-12087.
13. Tsukamoto, K.; Sahade, D. A.; Taniguchi, M.; Sawada, T.; Thiemann, T.; Mataka, S. Tetrahedron Lett. 1999, 40, 4691-4692.
14. Yaniamoto, G.; Oki, M. Bull. Chem. Soc. Jpn. 1990, 63, 3550-3559.
15. Seiders, T. J.; Elliott, E. L.; Grube, G. H.; Siegel, J. S. J. Am. Chem. Soc. 1999, 121, 7804-7813.
16. 3 520.1353.
17. (a) Kurland, R. J.; Rubin, M. B.; Wise, W. B. J. Chem. Phys. 1964, 40, 2426-2427.
18. (b) Sandstrom, J. Dynamic NMR Spectroscope; Academic: New York, 1982; pp 77-123.
19. 2, 96), 279 (100).
20. 2) = 0.1408, and S = 1.026 for 5085 unique reflections and 260 parameters.
21. (a) Otwinowski, Z.; Minor, W. Methods Enzymol. 1997, 276, 307-326.
22. (b) Sheldrick, G. M. SHELXTL, version 5; Siemens Analytical X-ray Instruments: Madison, WI, 1996.
23. Spek, A. L. J. Appl. Cryst. 2003, 36, 7-13.
24. Calculations were performed by using GAUSSIAN 98; the built-in default thresholds for wave function and gradient convergence were employed.
25. Pascal, R. A., Jr. J. Phys. Chem. A 2001, 105, 9040-9048.
26. Allen, F. H.; Kennard, O.; Taylor, R. Acc. Chem. Kes. 1983, 16, 146-153.
27. Only nonionic, nonorganometallic structures are included in this average.