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Undesired regioisomer was not observed. This regiochemical outcome is consistent with that of Asaoka's previous studies. Refer to ref 10a.
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32
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23044509809
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note
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On the basis of extensive spectroscopic studies on the isoxazoline 21, the configuration of isoxazoline 21 is likely to be 12R (12H-α), which is readily separable by flash column chromatography.
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33
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23044494182
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note
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Minor isomer of isoxazoline 21 was resistant to both reductive N-O bond cleavage and dehydration.
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