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European Journal of Organic Chemistry

Volumn , Issue 14, 2005, Pages 2881-2883

Iridium(I)-catalysed tandem hydrosilylation-protodesilylation of imines

(3) Field, Leslie D a Messerle, Barbara A b Rumble, Sarah L b

a UNIVERSITY OF SYDNEY (Australia)

b UNIVERSITY OF NEW SOUTH WALES (Australia)

Author keywords

Homogeneous catalysis; Hydrosilylation; Imines; Iridium; Solvent effects

Indexed keywords

EID: 22544487232 PISSN: 1434193X EISSN: None Source Type: Journal
DOI: 10.1002/ejoc.200500168 Document Type: Article

Times cited : (28)

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- note
- The Ir complex 1 (5.6 mg, 7.8 μmol) and the imine 3a (71 mg, 0.39 mmol) were dissolved in THF (2 mL) and stirred at 60°C in a stainless steel bomb under a hydrogen pressure of 120 psi for 20 min. The amine 4a was formed in quantitative yield (by NMR spectroscopy).

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