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13C NMR and GC-MS spectroscopies by comparison with the authentic samples.
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33
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20444461853
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note
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Under the same reaction conditions, the reaction of benzyl alcohol with fert-butyl alcohol afforded the corresponding benzyl tert-butyl ether in only 31% GC yield. In this case, isobutylene formed from the dehydration of tert-butyl alcohol, and the conversion of tert-butyl alcohol reached 82%.
-
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34
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and references therein
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For the similar oxidation of Be(III) and Re(V) by oxygen, see: (a) Smith, K. J.; Ondracek, A. L.; Gruhn, N. E.; Lichtenberger, D. L.; Fanwick, P. E.; Walton, R. A. Inorg. Chim. Acta 2000, 300/302, 23.
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