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19744378193
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note
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18]·2tol after 2 days (ca. 56% crystalline yield).
-
-
-
-
27
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-
19744375560
-
-
note
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3, Z = 4, R1/wR2 = 4.97/12.02% for the observed data (1 ≥ 2σ(1)), R1/wR2 = 7.79/13.28% for all data.
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29
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0001460917
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19744371082
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note
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4-.
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33
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0036033824
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0004133516
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Gaussian, Inc.: Piltsburgh, PA
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Calculations were performed with the Becke three-parameter density functional and the Lee-Yang-Parr correlation functional (B3LYP) in conjunction with the 3-21G basis set: Frisch, M. J. et al. Gaussian 98, revision A. 11.3; Gaussian, Inc.: Piltsburgh, PA, 2002.
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Gaussian 98, Revision A. 11.3
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Jones, P.G.6
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39
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19744377916
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note
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Electrospray mass spectra were recorded from 10 to 20 μM solutions on a Micromass Quattro-LC triple quadrupole mass spectrometer (125 °C source temperature, 150 °C desolvation temperature, 3 kV capillary voltage, and 25 V cone voltage).
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