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Although previously reported, the synthesis of 5 is presented here with additional characterization. For details, see: Ilhan, F.; Tyson, D. S.; Meador, M. A. Chem. Mater. 2004, 16, 2978-2980.
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18744395430
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note
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These values of end cap percent would correspond to a formulated molecular weight of 40K and 200K, respectively, if the acrylate did not self-polymerize.
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17
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18744392192
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note
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Due to limited quantities of the bis(o-methylphenyl ketone)s and the fundamental nature (i.e. proof-of-concept approach) of the experimental design, our objective was to minimize the number of runs while maintaining statistical significance.
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