Determination of toxic cyclic heptapeptides by liquid chromatography with detection using ultra-violet, protein phosphatase assay and tandem mass spectrometry

Chemosphere

Volumn 55, Issue 10, 2004, Pages 1395-1402

  Ortea, Paloma Muñiz ^a   Allis, Orla ^a   Healy, Brendan M ^a   Lehane, Mary ^a   Shuilleabháin, Aine Ní ^b   Furey, Ambrose ^a   James, Kevin J ^a  

^a Munster Technological University   (Ireland)

^b Northern Regional Fisheries Board   (Ireland)

Author keywords

Hepatotoxins; Ion trap mass spectrometry; Microcystins; Nodularin

Indexed keywords

ACETONITRILE; BIOASSAY; DISSOCIATION; ENZYMES; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PHOTODIODES; TOXIC MATERIALS; ULTRAVIOLET RADIATION;

SOLID-PHASE EXTRACTION; TOXINS;

POLYPEPTIDES;

ACETONITRILE; BACTERIAL TOXIN; CYANOGINOSIN; HEPTAPEPTIDE; NODULARIN; PHOSPHOPROTEIN PHOSPHATASE;

BIOCHEMICAL COMPOSITION;

ANALYTIC METHOD; ARTICLE; CALIBRATION; COLLISIONALLY ACTIVATED DISSOCIATION; CONTROLLED STUDY; ENZYME ASSAY; FRACTIONATION; LAKE ECOSYSTEM; MICROCYSTIS; NONHUMAN; RELIABILITY; REPRODUCIBILITY; REVERSED PHASE LIQUID CHROMATOGRAPHY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; ULTRAVIOLET SPECTROSCOPY; WATER POLLUTION;

CHROMATOGRAPHY, LIQUID; CYANOBACTERIA; FRESH WATER; IRELAND; MICROCYSTINS; PEPTIDES, CYCLIC; PHOSPHOPROTEIN PHOSPHATASE; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; ULTRAVIOLET RAYS;

MICROCYSTIS; MICROCYSTIS SP.; VIOLA (ANGIOSPERM);

EID: 1842687466     PISSN: 00456535     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chemosphere.2003.11.025     Document Type: Article

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