Synthesis, characterization and crystal structure of a monomeric and a macrocyclic copper (II) complex with a large cavity using benzylacetylacetone ligand

Inorganica Chimica Acta

Volumn 357, Issue 7, 2004, Pages 1991-1996

  Dey, Subrata Kumar ^a   Bag, Bappaditya ^a   Zhou, Zhongyuan ^b   Chan, Albert S C ^b   Mitra, Samiran ^a  

^a JADAVPUR UNIVERSITY   (India)

^b HONG KONG POLYTECHNIC UNIVERSITY   (Hong Kong)

Author keywords

4, 4 Bipyridine; Benzylacetylacetone; Crystal structures; Cu(II) monomeric and macrocyclic complexes

Indexed keywords

CHELATION; CHROMIUM COMPOUNDS; CRYSTAL STRUCTURE; ENERGY DISPERSIVE X RAY ANALYSIS; GEOMETRY; LIGANDS; SPECTROSCOPIC ANALYSIS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

BENZYLACETYLACETONE; BIPYRIDINES; MACROCYCLIC COMPLEX; MONONUCLEAR COMPLEXES; SQUARE PLANAR GEOMETRY; SQUARE-PYRAMIDAL GEOMETRY; TETRANUCLEAR COMPLEXES; THERMOGRAVIMETRIC STUDIES;

COPPER COMPOUNDS;

ACETIC ACID DERIVATIVE; BIPYRIDINE DERIVATIVE; COPPER COMPLEX; LIGAND; MACROCYCLIC COMPOUND;

ARTICLE; CRYSTAL STRUCTURE; DECOMPOSITION; GEOMETRY; INFRARED SPECTROSCOPY; PHYSICAL CHEMISTRY; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; SYNTHESIS; THERMOGRAVIMETRY;

EID: 1842636675     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ica.2003.12.014     Document Type: Article

References (33)

1. Curlucci L., Ciani G., Proserpio D.M., Sironi A. J. Am. Chem. Soc. 117:1995;4562.
2. Curlucci L., Ciani G., Proserpio D.M., Sironi A. Angew. Chem., Int. Ed. Engl. 34:1995;1895.
3. Yaghi O.M., Li H., Groy T.L. Inorg. Chem. 36:1997;4292.
4. Blake A.J., Champness N.R., Khlobystv A.N., Parsons S., Schroder M. Angew. Chem., Int. Ed. Engl. 39:2000;2317.
5. Olenyuk B., Fechtenkotter A., Stang J. J. Chem. Soc., Dalton Trans. 1998;1707.
6. They have interpenetrating structures possessing no inner cavity. For M = Zn, see the following. Gable R.W., Hoskins B.F., Robson R. J. Chem. Soc., Chem. Commun. 1990;1667.
7. For M = Cu and Cd, see the following. Robson R., Abrahams B.F., Batten S.R., Gable R.W., Oskins B.F., Liu J. Bein T. Supramolecular Architecture. ACS Symposium Series. vol. 499:1992;American Chemical Society, Washington, DC. (Chapter 19).
8. For Ni, see the following. Choudhury C.R., Dey S.K., Sen S., Bag B., Mitra S., Gramlich V. Z. Naturforsch., Teil B. 2002;1191.
9. Desiaraju G.R. Crystal Engineering: Design of Organic Solids. 1989;Elsevier, Amsterdam.
10. Ermer O. J. Am. Chem. Soc. 110:1988;3747.
11. Ermer O., Eling A. J. Chem. Soc. Perkin Trans. 1994;925. and references therein.
12. Venkataraman D., Lee S., Zhang J., Moore J.S. Nature. 371:1994;591.
13. Sheldrick G.M. Acta Crystallogr., Sect. A. 46:1990;457.
14. Sheldrick G.M. SHELXL-97 Program for Crystal Structure Refinement. 1997;University of Göttingen, Germany.
15. Dey S.K., Bag B., Malik K.M.A., El Fallah M.S., Ribas J., Mitra S. Inorg. Chem. 42:2003;4029.
16. Colacio E., Domínguez-Vera J.M., Ghazi M., Kivekäs R., Klinga M., Moreno J.M. Eur. J. Inorg. Chem. 1999;441.
17. Sen S., Saha M.K., Gupta T., Karmakar A.K., Kundu P., Mitra S., Hursthouse M.B., Malik K.M.A. J. Chem. Crystallogr. 28:1998;771. and references therein.
18. Nakamoto K. Infrared and Raman Spectra of Inorganic and Coordination Compounds. third ed. 1978;Interscience-Wiley, New York. p. 233.
19. Suzuki M., Uehara A. Bull. Chem. Soc. Jpn. 57:1984;3134.
20. Hathaway B.J., Tomlinson A.A.G. Coord. Chem. Rev. 5:1970;1.
21. Brown S.J., Stephen D.W., Mascharak P.K. J. Am. Chem. Soc. 110:1988;1996.
22. Chevez F.A., Olmstead M.M., Mascharak P.K. Inorg. Chim. Acta. 269:1998;269.
23. Dey S.K., Choudhury C.R., Dey S.P., Dey D.K., Mondal N., Mahalli S.O.G., Malik K.M.A., Mitra S. J. Chem. Res. 2002;496.
24. Escuer A., Font-Bardia M., Penalba F., Solans X., Vicente R. Inorg. Chim. Acta. 286:1999;189.
25. Hunter C.A. Angew. Chem. 107:1995;1181.
26. Hunter C.A. Angew. Chem., Int. Ed. Engl. 34:1995;1079.
27. Fujita M., Yazaki J., Ogura K. J. Am. Chem. Soc. 112:1990;5645.
28. Stang P.J., Cao D.H. J. Am. Chem. Soc. 116:1994;4981.
29. Slone R.V., Yoon D.I., Calhoun R.M., Hupp J.T. J. Am. Chem. Soc. 117:1995;11813.
30. Stang P.J., Olenyuk B. Angew. Chem. 108:1996;798.
31. Stang P.J., Olenyuk B. Angew. Chem., Int. Ed. Engl. 35:1996;732.
32. Alternate motifs are possible for assembly of "T-shape" moieties: Robinson F., Zaworotko M.J. J. Chem. Soc., Chem. Commun. 1995;2413.
33. Yaghi O.M., Li H. J. Am. Chem. Soc. 118:1996;295.