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Volumn 2, Issue 6, 2004, Pages 852-857

5-Pyrimidylboronic acid and 2-methoxy-5-pyrimidylboronic acid: New heteroarylpyrimidine derivatives via Suzuki cross-coupling reactions

Author keywords

[No Author keywords available]

Indexed keywords

CATALYSIS; CRYSTAL STRUCTURE; ELECTRON TRANSITIONS; HYDROGEN BONDS; REACTION KINETICS; X RAY CRYSTALLOGRAPHY;

EID: 1842586937     PISSN: 14770520     EISSN: None     Source Type: Journal    
DOI: 10.1039/b314624n     Document Type: Article
Times cited : (45)

References (50)
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    • T. Wang, Z. Zhang, N. Meanwell, J. F. Kadow and Z. Yin, WO 02/062423/ 2002
    • (b) T. Wang, Z. Zhang, N. Meanwell, J. F. Kadow and Z. Yin, WO 02/062423/ 2002.
  • 13
    • 2042507954 scopus 로고
    • Reviews: (a) N. Miyaura and A. Suzuki, Chem. Rev., 1995, 95, 2457; (b) S. P. Stanforth, Tetrahedron, 1998, 54, 263; (c) A. Suzuki, in Metal-Catalyzed Cross-Coupling Reactions, eds F. Diederich and P. J. Stang, Wiley-VCH, Weinheim, Germany, 1998, ch. 2; (d) For a review of new palladacyclic catalysts for Suzuki reactions see: R. B. Bedford, Chem. Commun., 2003, 1787.
    • (1995) Chem. Rev. , vol.95 , pp. 2457
    • Miyaura, N.1    Suzuki, A.2
  • 14
    • 0032518829 scopus 로고    scopus 로고
    • Reviews: (a) N. Miyaura and A. Suzuki, Chem. Rev., 1995, 95, 2457; (b) S. P. Stanforth, Tetrahedron, 1998, 54, 263; (c) A. Suzuki, in Metal-Catalyzed Cross-Coupling Reactions, eds F. Diederich and P. J. Stang, Wiley-VCH, Weinheim, Germany, 1998, ch. 2; (d) For a review of new palladacyclic catalysts for Suzuki reactions see: R. B. Bedford, Chem. Commun., 2003, 1787.
    • (1998) Tetrahedron , vol.54 , pp. 263
    • Stanforth, S.P.1
  • 15
    • 1842502128 scopus 로고    scopus 로고
    • eds F. Diederich and P. J. Stang, Wiley-VCH, Weinheim, Germany, ch. 2
    • Reviews: (a) N. Miyaura and A. Suzuki, Chem. Rev., 1995, 95, 2457; (b) S. P. Stanforth, Tetrahedron, 1998, 54, 263; (c) A. Suzuki, in Metal-Catalyzed Cross-Coupling Reactions, eds F. Diederich and P. J. Stang, Wiley-VCH, Weinheim, Germany, 1998, ch. 2; (d) For a review of new palladacyclic catalysts for Suzuki reactions see: R. B. Bedford, Chem. Commun., 2003, 1787.
    • (1998) Metal-catalyzed Cross-coupling Reactions
    • Suzuki, A.1
  • 16
    • 0042905927 scopus 로고    scopus 로고
    • Reviews: (a) N. Miyaura and A. Suzuki, Chem. Rev., 1995, 95, 2457; (b) S. P. Stanforth, Tetrahedron, 1998, 54, 263; (c) A. Suzuki, in Metal-Catalyzed Cross-Coupling Reactions, eds F. Diederich and P. J. Stang, Wiley-VCH, Weinheim, Germany, 1998, ch. 2; (d) For a review of new palladacyclic catalysts for Suzuki reactions see: R. B. Bedford, Chem. Commun., 2003, 1787.
    • (2003) Chem. Commun. , pp. 1787
    • Bedford, R.B.1
  • 35
  • 36
    • 1842502127 scopus 로고    scopus 로고
    • Seal Sands Chemicals Ltd., personal communication
    • Impure product 2 was also obtained under the conditions described in ref. 13e in independent studies in another laboratory: Seal Sands Chemicals Ltd., personal communication. The isolated product may be a mixture of the boroxin trimer and varying amounts of hydrates.
    • Parry, P.R.1
  • 41
    • 0032119961 scopus 로고    scopus 로고
    • Reviews, (a) M. Thelakkat and H.-W Schmidt, Polym. Adv. Technol., 1998, 9, 429; (b) Y. Shirota, J. Mater. Chem., 2000, 10, 1; (c) U. Mitschke and P. Bäuerle, J. Mater. Chem., 2000, 10, 1471.
    • (1998) Polym. Adv. Technol. , vol.9 , pp. 429
    • Thelakkat, M.1    Schmidt, H.-W.2
  • 42
    • 0034031562 scopus 로고    scopus 로고
    • Reviews, (a) M. Thelakkat and H.-W Schmidt, Polym. Adv. Technol., 1998, 9, 429; (b) Y. Shirota, J. Mater. Chem., 2000, 10, 1; (c) U. Mitschke and P. Bäuerle, J. Mater. Chem., 2000, 10, 1471.
    • (2000) J. Mater. Chem. , vol.10 , pp. 1
    • Shirota, Y.1
  • 43
    • 0033927513 scopus 로고    scopus 로고
    • Reviews, (a) M. Thelakkat and H.-W Schmidt, Polym. Adv. Technol., 1998, 9, 429; (b) Y. Shirota, J. Mater. Chem., 2000, 10, 1; (c) U. Mitschke and P. Bäuerle, J. Mater. Chem., 2000, 10, 1471.
    • (2000) J. Mater. Chem. , vol.10 , pp. 1471
    • Mitschke, U.1    Bäuerle, P.2
  • 47
    • 1842554374 scopus 로고    scopus 로고
    • 5-Bromo-2-methoxypyrimmidine is commercially available from Frontier Scientfic (ww.frontiersci.com). its synthesis is described in refernce 3b, by the reaction of 5-bromo-2-chloropumidine (ref. 4c) with sodium metoxide (0.5 M in methanol) at 20° for 1 day
  • 50
    • 0004150157 scopus 로고    scopus 로고
    • Bruker AXS, Madison, Wisconsin, USA
    • SHELXTL, version 5.1; Bruker AXS, Madison, Wisconsin, USA, 1997.
    • (1997) SHELXTL, Version 5.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.