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Volumn 40, Issue 4, 2005, Pages 494-502

Characterization of chemically modified steroids for doping control purposes by electrospray ionization tandem mass spectrometry

Author keywords

Designer steroids; Doping; Electrospray ionization; Fragmentation; Mass spectrometry

Indexed keywords

DISSOCIATION; DOPING (ADDITIVES); DRUG PRODUCTS; IONIZATION; MASS SPECTROMETERS; SYNTHESIS (CHEMICAL);

EID: 18344374877     PISSN: 10765174     EISSN: None     Source Type: Journal    
DOI: 10.1002/jms.820     Document Type: Article
Times cited : (72)

References (33)
  • 3
    • 0035983385 scopus 로고    scopus 로고
    • Detection of norbolethone, an anabolic steroid never marketed, in athletes' urine
    • Catlin DH, Ahrens BD, Kucherova Y. Detection of norbolethone, an anabolic steroid never marketed, in athletes' urine. Rapid Commun. Mass Spectrom. 2002; 16: 1273.
    • (2002) Rapid Commun. Mass Spectrom. , vol.16 , pp. 1273
    • Catlin, D.H.1    Ahrens, B.D.2    Kucherova, Y.3
  • 4
    • 3142599890 scopus 로고    scopus 로고
    • Athlete's 'designer steroid' leads to widening scandal
    • Kondro W. Athlete's 'designer steroid' leads to widening scandal. Lancet 2003; 362: 1466.
    • (2003) Lancet , vol.362 , pp. 1466
    • Kondro, W.1
  • 5
    • 0242331737 scopus 로고    scopus 로고
    • Drugs bust reveals athletes' secret steroid
    • Knight J. Drugs bust reveals athletes' secret steroid. Nature 2003; 425: 752.
    • (2003) Nature , vol.425 , pp. 752
    • Knight, J.1
  • 6
    • 0642342092 scopus 로고    scopus 로고
    • Drugs in sport: No dope
    • Knight J. Drugs in sport: no dope. Nature 2003; 426: 114.
    • (2003) Nature , vol.426 , pp. 114
    • Knight, J.1
  • 8
    • 0035810852 scopus 로고    scopus 로고
    • Screening, confirmation and quantification of diuretics in urine for doping control analysis by high-performance liquid chromatography-atmospheric pressure ionisation tandem mass spectrometry
    • Thieme D, Grosse J, Lang R, Müller RK, Wahl A. Screening, confirmation and quantification of diuretics in urine for doping control analysis by high-performance liquid chromatography-atmospheric pressure ionisation tandem mass spectrometry. J. Chromatogr. B 2001; 757: 49.
    • (2001) J. Chromatogr. B , vol.757 , pp. 49
    • Thieme, D.1    Grosse, J.2    Lang, R.3    Müller, R.K.4    Wahl, A.5
  • 9
    • 0034820973 scopus 로고    scopus 로고
    • High speed determination of beta-receptor blocking agents in human urine by liquid chromatography/tandem mass spectrometry
    • Thevis M, Opfermann G, Schänzer W. High speed determination of beta-receptor blocking agents in human urine by liquid chromatography/tandem mass spectrometry. Biomed. Chromatogr. 2001; 15: 393.
    • (2001) Biomed. Chromatogr. , vol.15 , pp. 393
    • Thevis, M.1    Opfermann, G.2    Schänzer, W.3
  • 10
    • 1542375446 scopus 로고    scopus 로고
    • Screening of free 17-alkyl-substituted anabolic steroids in human urine by liquid chromatography-electrospray ionization tandem mass spectrometry
    • Leinonen A, Kuuranne T, Kotiaho T, Kostiainen R. Screening of free 17-alkyl-substituted anabolic steroids in human urine by liquid chromatography-electrospray ionization tandem mass spectrometry. Steroids 2004; 69: 101.
    • (2004) Steroids , vol.69 , pp. 101
    • Leinonen, A.1    Kuuranne, T.2    Kotiaho, T.3    Kostiainen, R.4
  • 11
    • 0042836931 scopus 로고    scopus 로고
    • Validation of a screening method for corticosteroids in doping analysis by liquid chromatography/tandem mass spectrometry
    • Deventer K, Delbeke FT. Validation of a screening method for corticosteroids in doping analysis by liquid chromatography/tandem mass spectrometry. Rapid Commun. Mass Spectrom. 2003; 17: 2107.
    • (2003) Rapid Commun. Mass Spectrom. , vol.17 , pp. 2107
    • Deventer, K.1    Delbeke, F.T.2
  • 12
    • 0345547402 scopus 로고    scopus 로고
    • Liquid chromatography/electrospray ionization tandem mass spectrometric screening and confirmation methods for β2-agonists in human or equine urine
    • Thevis M, Opfermann G, Schänzer W. Liquid chromatography/ electrospray ionization tandem mass spectrometric screening and confirmation methods for β2-agonists in human or equine urine. J. Mass Spectrome. 2003; 38: 1197.
    • (2003) J. Mass Spectrome. , vol.38 , pp. 1197
    • Thevis, M.1    Opfermann, G.2    Schänzer, W.3
  • 13
    • 0003229802 scopus 로고
    • Mass spectrometry in structural and stereochemical problems. XLVIII. A study of the hydrogen transfer reactions accompanying fragmentation processes of 1-keto steroids. Synthesis of deuterated 5α-androstan-1-ones
    • Powell H, Williams DH, Budzikiewicz H, Djerassi C. Mass spectrometry in structural and stereochemical problems. XLVIII. A study of the hydrogen transfer reactions accompanying fragmentation processes of 1-keto steroids. Synthesis of deuterated 5α-androstan-1-ones. J. Am. Chem. Soc. 1964; 86: 2623.
    • (1964) J. Am. Chem. Soc. , vol.86 , pp. 2623
    • Powell, H.1    Williams, D.H.2    Budzikiewicz, H.3    Djerassi, C.4
  • 14
    • 18344371044 scopus 로고
    • Mass spectrometry in structural and stereochemical problems. LI. Mass spectral end enolization studies on 7-keto-5α-androstanes
    • Beugelmans R, Shapiro RH, Durham LJ, Williams DH, Budzikiewicz H, Djerassi C. Mass spectrometry in structural and stereochemical problems. LI. Mass spectral end enolization studies on 7-keto-5α-androstanes. J. Am. Chem. Soc. 1964; 86: 2832.
    • (1964) J. Am. Chem. Soc. , vol.86 , pp. 2832
    • Beugelmans, R.1    Shapiro, R.H.2    Durham, L.J.3    Williams, D.H.4    Budzikiewicz, H.5    Djerassi, C.6
  • 15
    • 0000289654 scopus 로고
    • Mass spectrometry in structural and stereochemical problems. LIII. Fragmentation and hydrogen transfer reactions of a typical 3-keto steroid, 5α-androstan-3-one
    • Shapiro RH, Williams DH, Budzikiewicz H, Djerassi C. Mass spectrometry in structural and stereochemical problems. LIII. Fragmentation and hydrogen transfer reactions of a typical 3-keto steroid, 5α-androstan-3-one. J. Am. Chem. Soc. 1964; 86: 2837.
    • (1964) J. Am. Chem. Soc. , vol.86 , pp. 2837
    • Shapiro, R.H.1    Williams, D.H.2    Budzikiewicz, H.3    Djerassi, C.4
  • 16
    • 0001379163 scopus 로고
    • Mass spectrometry in structural and stereochemical problems. XCl. The electron impact induced elimination of water from 3-hydroxy steroids
    • Karliner J, Budzikiewicz H, Djerassi C. Mass spectrometry in structural and stereochemical problems. XCl. The electron impact induced elimination of water from 3-hydroxy steroids. J. Org. Chem. 1966; 31: 710.
    • (1966) J. Org. Chem. , vol.31 , pp. 710
    • Karliner, J.1    Budzikiewicz, H.2    Djerassi, C.3
  • 19
    • 0034789694 scopus 로고    scopus 로고
    • Mass spectrometry of steroid glucuronide conjugates. 11-Electron impact fragmentation of 3-keto-4-en-and 3-keto-5alpha-steroid-17-o-beta glucuronides and 5alpha-steroid-3alpha,17beta-diol 3- And 17-glucuronides
    • Thevis M, Opfermann G, Schmickler H, Schänzer W. Mass spectrometry of steroid glucuronide conjugates. 11-Electron impact fragmentation of 3-keto-4-en-and 3-keto-5alpha-steroid-17-o-beta glucuronides and 5alpha-steroid-3alpha,17beta-diol 3- and 17-glucuronides. J. Mass Spectrom. 2001; 36: 998.
    • (2001) J. Mass Spectrom. , vol.36 , pp. 998
    • Thevis, M.1    Opfermann, G.2    Schmickler, H.3    Schänzer, W.4
  • 20
    • 17044374511 scopus 로고
    • Massenspektren und Stereochemie von Hydroxyverbindungen, 1. Mitt.: Hydroxysteroide
    • Egger H, Spiteller G. Massenspektren und Stereochemie von Hydroxyverbindungen, 1. Mitt.: Hydroxysteroide. Monatsh. Chem. 1966; 97: 579.
    • (1966) Monatsh. Chem. , vol.97 , pp. 579
    • Egger, H.1    Spiteller, G.2
  • 21
    • 18344374564 scopus 로고
    • Studies in mass spectrometry stereochemistry and elimination reactions of hydroxy and acetoxy compounds
    • Macdonald CG, Shannon JS, Sugowdz G. Studies in mass spectrometry stereochemistry and elimination reactions of hydroxy and acetoxy compounds. Tetrahedron Lett. 1963; 4: 807.
    • (1963) Tetrahedron Lett. , vol.4 , pp. 807
    • Macdonald, C.G.1    Shannon, J.S.2    Sugowdz, G.3
  • 22
    • 18344379213 scopus 로고
    • Organic ions in the gas phase. XIV. Loss of water from primary alcohols under electron impact
    • Meyerson S, Leitch LC. Organic ions in the gas phase. XIV. Loss of water from primary alcohols under electron impact. J. Am. Chem. Soc. 1964; 86: 2555.
    • (1964) J. Am. Chem. Soc. , vol.86 , pp. 2555
    • Meyerson, S.1    Leitch, L.C.2
  • 24
    • 0036683499 scopus 로고    scopus 로고
    • Mass spectrometric behavior of thiazide-based diuretics after electrospray ionization and collision-induced dissociation
    • Thevis M, Schmickler H, Schänzer W. Mass spectrometric behavior of thiazide-based diuretics after electrospray ionization and collision-induced dissociation. Anal. Chem. 2002; 74: 3802.
    • (2002) Anal. Chem. , vol.74 , pp. 3802
    • Thevis, M.1    Schmickler, H.2    Schänzer, W.3
  • 26
    • 0035119347 scopus 로고    scopus 로고
    • Collision-induced fragmentation of deprotonated methoxylated flavonoids, obtained by electrospray ionization mass spectrometry
    • Justesen U. Collision-induced fragmentation of deprotonated methoxylated flavonoids, obtained by electrospray ionization mass spectrometry. J. Mass Spectrom. 2001; 36: 169.
    • (2001) J. Mass Spectrom. , vol.36 , pp. 169
    • Justesen, U.1
  • 27
    • 0034845739 scopus 로고    scopus 로고
    • Tandem mass spectrum of a farnesyltransferase inhibitor-gas phase rearrangements involving imidazole
    • Qin X-Z. Tandem mass spectrum of a farnesyltransferase inhibitor-gas phase rearrangements involving imidazole. J. Mass Spectrom. 2001; 36: 911.
    • (2001) J. Mass Spectrom. , vol.36 , pp. 911
    • Qin, X.-Z.1
  • 28
    • 0033026017 scopus 로고    scopus 로고
    • Electrospray collision-induced dissociation of testosterone and testosterone hydroxy analogs
    • Williams TM, Kind AJ, Houghton E, Hill DW. Electrospray collision-induced dissociation of testosterone and testosterone hydroxy analogs. J. Mass Spectrom. 1999; 34: 206.
    • (1999) J. Mass Spectrom. , vol.34 , pp. 206
    • Williams, T.M.1    Kind, A.J.2    Houghton, E.3    Hill, D.W.4
  • 30
    • 15444353731 scopus 로고
    • Anti-androgenic activity of 17,17-dimethyl-18-norandrost-13-enes
    • Segaloff A, Gabbard RB. Anti-androgenic activity of 17,17-dimethyl-18- norandrost-13-enes. Steroids 1964; 4: 433.
    • (1964) Steroids , vol.4 , pp. 433
    • Segaloff, A.1    Gabbard, R.B.2
  • 31
    • 37049151429 scopus 로고
    • The synthesis of compounds related to sterols, bile acids, and oestrus-producing hormones. Part VI. Experimental evidence of the complete structure of oestrin, equilin, and equilenin
    • Cohen A, Cook JW, Hewett CL. The synthesis of compounds related to sterols, bile acids, and oestrus-producing hormones. Part VI. Experimental evidence of the complete structure of oestrin, equilin, and equilenin. J. Chem. Soc. 1935; 445.
    • (1935) J. Chem. Soc. , pp. 445
    • Cohen, A.1    Cook, J.W.2    Hewett, C.L.3
  • 32
    • 0000738023 scopus 로고
    • Retropinacol rearrangement of estradiol 3-methyl ether
    • Johns WF. Retropinacol rearrangement of estradiol 3-methyl ether. J. Org. Chem. 1961; 26: 4583.
    • (1961) J. Org. Chem. , vol.26 , pp. 4583
    • Johns, W.F.1
  • 33
    • 0026445656 scopus 로고
    • 17-Epimerization of 17 alpha-methyl anabolic steroids in humans: Metabolism and synthesis of 17 alpha-hydroxy-17β-methyl steroids
    • Schänzer W, Opfermann G, Donike M. 17-Epimerization of 17 alpha-methyl anabolic steroids in humans: metabolism and synthesis of 17 alpha-hydroxy-17β-methyl steroids. Steroids 1992; 57: 537.
    • (1992) Steroids , vol.57 , pp. 537
    • Schänzer, W.1    Opfermann, G.2    Donike, M.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.