Assisted crystallization of organometallic cations by interplay with inorganic anionic clusters units: Synthesis and characterizations of the [Cp*(dppe)Fe-NCMe]2·M6L14 series (M6L14 = cluster unit: [Re6S6Br 8]2-, [Mo6Br14]2-

European Journal of Inorganic Chemistry

Volumn , Issue 5, 2005, Pages 919-928

  Pilet, Guillaume ^a,b,c   Kirakci, Kaplan ^a   De Montigny, Frédéric ^e   Cordier, Stéphane ^a   Lapinte, Claude ^d   Perrin, Christiane ^a   Perrin, André ^a  

^a Laboratoire de Chimie du Solide et Inorganique Moleculaire de Rennes   (France)

^b STOCKHOLM UNIVERSITY   (Sweden)

^c UNIVERSITÉ CLAUDE BERNARD LYON 1   (France)

^d UMR 6509 Organometalliques et Catalyse Chimie et Electrochimie Moleculaires   (France)

^e NONE

Author keywords

Hybrid compounds; Inorganic organometallic chemistry; Iron; M6L14 units; Molybdenum octahedral clusters; Rhenium; Single crystal structures

Indexed keywords

CESIUM COMPOUNDS; IRON; NEGATIVE IONS; ORGANOMETALLICS; POSITIVE IONS; RHENIUM; SINGLE CRYSTALS;

ANIONIC CLUSTERS; CLUSTER UNITS; HYBRID COMPOUNDS; INORGANIC ORGANOMETALLIC CHEMISTRY; INORGANICS; M6L14 UNIT; MOLYBDENUM OCTAHEDRAL CLUSTER; OCTAHEDRAL CLUSTERS; ORGANOMETALLIC CHEMISTRY; SINGLE-CRYSTAL STRUCTURE;

MOLYBDENUM;

ACETONITRILE; ANION; CATION; CESIUM CHLORIDE; CHLORIDE ION; MOLYBDENUM; ORGANOMETALLIC COMPOUND; RHENIUM;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; INFRARED SPECTROSCOPY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PRECIPITATION; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY DIFFRACTION;

EID: 16644393797     PISSN: 14341948     EISSN: None     Source Type: Journal    
DOI: 10.1002/ejic.200400798     Document Type: Article

References (24)

1. A. Perrin, M. Sergent, New J. Chem. 1988, 12, 337.
2. A. Perricone, A. Slougui, A. Perrin, Solid State Sci. 1999, 1, 657.
3. J. P. Gabriel, K. Boubekeur, S. Uriel, P. Batail, Chem. Rev. 2001, 101, 2037.
4. A. Perrin, C. Perrin, M. Sergent, J. Less-Common. Met. 1988, 137, 241.
5. C. Perrin, J. Alloys Compd. 1997, 262-263, 10, and references cited therein.
6. H. Schäfer, H. G. von Schnering, Angew. Chem. 1964, 76, 833.
7. R. Chevrel, M. Sergent, "Superconductivity in Ternary Compounds", in Topics in Current Physics (Eds.: Ø. Fischer, M. P. Maple), Springer Verlag, Berlin, Heidelberg, New York, 1982.
8. Metal Clusters in Chemistry, vol. II (Eds.: P. Braunstein, L. A. Oro, P. R. Raithby), Wiley-VCH, Weinheim, 1999.
9. J. M. Tarascon, F. J. Di Salvo, D. W. Murphy, G. W. Hull, E. A. Rietman, S. V. Waszczak, J. Solid State Chem. 1984, 54, 104.
10. H. D. Selby, B. K. Roland, Z. Zheng, Acc. Chem. Res. 2003, 36, 933.
11. M. W. Willer, J. R. Long, C. C. McLauhan, R. Holm, Inorg. Chem. 1998, 37, 328.
12. Nonius, COLLECT, DENZO, SCALEPACK, SORTAV: KappaCCD Program Package, Nonius B. V., Delft, The Netherlands, 1999.
13. J. De Meulenaar, H. Tompa, Acta Cryslallogr., Sect A 1965, 19, 1014.
14. G. Cascarano, A. Altomare, C. Giacovazzo, A. Guagliardi, A. G. G. Moliterni, D. Siliqi, M. C. Burla, G. Polidori, M. Camalli, Acta Crystallogr., Sect A 1996, 52, C-79.
15. D. J. Watkin, C. K. Prout, J. R. Carruthers, P. W. Betteridge, CRYSTAL, Chemical Crystallography Laboratory, Oxford, UK, 1999, issue 11.
16. A. Slougui, A. Perrin, M. Sergent, J. Solid State Chem. 1999. 147, 358.
17. J. Ruiz, D. Astruc, J.-P. Bideau, M. Cotrait, Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1990, 46, 2367.
18. F. Paul, C. Lapinte, Coord. Chem. Rev. 1998, 178-180, 427.
19. R. Denis, L. Toupet, F. Paul, C. Lapinte, Organometallics 2000, 19, 4240.
20. K. Costuas, F. Paul, L. Toupet, J.-F. Halet, C. Lapinte, Organometallics 2004, 23, 2053.
21. C. Roger, P. Hamon, L. Toupet, H. Rabaâ, J.-Y. Saillard, J.-R. Hamon, C. Lapinte, Organometallics 1991, 10, 1045.
22. G. Pilet, PhD Dissertation, Rennes, France, 2003.
23. K. Kirakci, S. Cordier, C. Perrin, Z. Anorg. Allgem. Chem., in press.
24. D. Catheline, D. Astruc, Organometallics 1984, 3, 1094.