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Volumn , Issue 4, 2004, Pages 726-728

Synthesis of 2H-labelled α-azidoisobutyryl chloride (D6-Azib-Cl) as 2H6-Aib equivalent building block in peptide synthesis

Author keywords

Azido acids; Bioorganic chemistry; Deuterium; Isotopic labelling; Peptides

Indexed keywords

2 AMINO 2 METHYLPROPIONIC ACID; ACETONE; ALPHA AZIDOISOBUTYRYL CHLORIDE; CYANOHYDRIN; DEUTERIUM; POLYPEPTIDE ANTIBIOTIC AGENT; UNCLASSIFIED DRUG;

EID: 1642403511     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2004-817748     Document Type: Article
Times cited : (10)

References (26)
  • 2
    • 2242420941 scopus 로고    scopus 로고
    • Jost, M.; Greie, J.-C.; Stemmer, N.; Wilking, S. D.; Altendorf, K.; Sewald, N. Angew. Chem. Int. Ed. 2002, 41, 4267; Angew. Chem. 2002, 114, 4438.
    • (2002) Angew. Chem. , vol.114 , pp. 4438
  • 7
    • 0031576691 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 12100
    • Tolbert, T.J.1    Williamson, J.R.2
  • 8
    • 18444416796 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (2002) Conc. Magn. Res. , vol.14 , pp. 1
    • Meissner, A.1    Sörensen, O.W.2
  • 9
    • 0037354160 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (2003) J. Biomol. NMR , vol.25 , pp. 235
    • Gross, J.D.1    Gelev, V.M.2    Wagner, G.3
  • 10
    • 0037736544 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (2003) J. Magn. Res. , vol.160 , pp. 78
    • Reif, B.1    Griffin, R.G.2
  • 11
    • 0037463033 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (2003) Angew. Chem. Int. Ed. , vol.42 , pp. 864
    • Meyer, B.1    Peters, T.2
  • 12
    • 0346996643 scopus 로고    scopus 로고
    • Representative examples: (a) Tolbert, T. J.; Williamson, J. R. J. Am. Chem. Soc. 1997, 119, 12100. (b) Meissner, A.; Sörensen, O. W. Conc. Magn. Res. 2002, 14, 1. (c) Gross, J. D.; Gelev, V. M.; Wagner, G. J. Biomol. NMR 2003, 25, 235. (d) Reif, B.; Griffin, R. G. J. Magn. Res. 2003, 160, 78. (e) Meyer, B.; Peters, T. Angew. Chem. Int. Ed. 2003, 42, 864; Angew. Chem. 2003, 115, 890.
    • (2003) Angew. Chem. , vol.115 , pp. 890
  • 20
    • 1642348314 scopus 로고    scopus 로고
    • note
    • 1H NMR): 92%.
  • 21
    • 1642376078 scopus 로고    scopus 로고
    • note
    • R = 3.4 min (100%); MS: m/z = 116 (11%), 74 (87%), 46 (100%).
  • 25
    • 1642299474 scopus 로고    scopus 로고
    • note
    • -1] = 2934 (sst), 2858 (st), 2361, 2111 (st), 1627 (st), 1451, 1383, 1267; MS (EI, 70 eV): m/z = 89 (13%), 76 (32%).


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