One-dimensional void-space arrays constructed from a coordination polymer with bowl-like frameworks of cavitands

Chemical Communications

Volumn , Issue 9, 2005, Pages 1140-1142

  Tadokoro, Makoto ^a   Mizugaki, Shin ^a   Kozaki, Masatoshi ^a   Okada, Keiji ^a  

^a Osaka Prefecture University   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID ETHYL ESTER; COORDINATION COMPOUND; MANGANESE; POLYMER;

ARTICLE; CRYSTAL STRUCTURE; STRUCTURE ANALYSIS; SUPRAMOLECULAR CHEMISTRY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 15444368507     PISSN: 13597345     EISSN: None     Source Type: Journal    
DOI: 10.1039/b415374j     Document Type: Article

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15. o by full matrix least squares. C-F bond distances on two hexafluoroacetylacetonate ligands were restricted to 1.31 Å and each F atom using the distributed occupancy factors, C(81), C(83), C(86) and C(90) was fixed and excluded from the final refine. EtOAc molecules without the inclusion into the cavitands were also calculated isotropically to fix the respective atom positions and bond distances of C-O (1.45 Å), C=O (1.35 Å) and C-C (1.65 Å). CCDC 251793. See http://www.rsc.org/suppdata/ cc/b4/b415374j/ for crystallographic data in .cif or other electronic format.
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