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Volumn 7, Issue 4, 2005, Pages 653-656

Cyclocarbopalladation: Sequential cyclization and C-H activation/Stille cross-coupling in the Pd-5-exo-dig reaction

Author keywords

[No Author keywords available]

Indexed keywords

PALLADIUM;

EID: 14844352903     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol047537s     Document Type: Article
Times cited : (94)

References (18)
  • 17
    • 14844341846 scopus 로고    scopus 로고
    • (from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB21EZ. UK; fax: (+44) 1223-336-033; or deposit@ccdc.cam.ac.uk)
    • -3. Measurements were collected on a Kappa CCD diffractometer (Mo Kα, graphite monochromated, λ = 0.71073 Å). These structures were solved using direct methods. After refinement of the non-hydrogen atoms, difference Fourier maps revealed maxima of residual electron density close to positions expected for hydrogen atoms. Hydrogen atoms were introduced as fixed contributors at calculated positions (C-H = 0.95 A, B(H) = 1.3 Bequiv). Final difference maps revealed no significant maxima. All calculations were done using the Nonius OpenMoleN package. Neutral atom scattering factor coefficients and anomalous dispersion coefficients were taken from a standard source. CCDC 240661 (17) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB21EZ. UK; fax: (+44) 1223-336-033; or deposit@ccdc.cam.ac.uk).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.