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note
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2O/THF ratios were in a range from 0.2 to 0.3 (v/v) under current conditions.
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14744267613
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note
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A Hitachi H-800 transmission electron microscope with the accelerating voltage of 150 kV was used to observe the spheres. The size and size distribution of the colloidal spheres were also measured with a Marvern Zetasizer 3000 dynamic light scattering instrument equipped with a multi-τdigital time correlation, a 632 nm solid-state laser light source. The scattering angle used for the measurement was 90°, and the temperature was controlled at 25 °C.
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The Scanning Electron Microscopy (SEM) measurement was performed on a field emission microscope JEOL JSM-6301F, which was operated with an accelerating voltage of 5 kV. All of the samples prepared for SEM studies were coated with thin layers of carbon (≃5 nm in thickness) before the measurement.
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