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Volumn 46, Issue 12, 2005, Pages 2059-2062

The use of deep cavity tetraformyl calix[4]arenes in the synthesis of static and dynamic macrocyclic libraries

Author keywords

[No Author keywords available]

Indexed keywords

CALIXARENE; MACROCYCLIC COMPOUND; PEPTIDE;

EID: 14644399238     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2005.01.168     Document Type: Article
Times cited : (7)

References (25)
  • 17
    • 85030814952 scopus 로고    scopus 로고
    • note
    • 2O requires C, 69.41; H, 6.38
  • 22
    • 85030811980 scopus 로고    scopus 로고
    • note
    • 3 requires C, 68.83; H, 5.56; N 3.04
  • 23
    • 0025318611 scopus 로고
    • FAB-MS spectra of representative equimolar mixtures of tetra-imines revealed differences of relative intensities of the molecular ions within 20%, indicating that LSIMS-MS is in this case a valid technique for the analysis of structurally closely related compounds of comparable molecular weight. It is furthermore worth noting that the library components could not be sufficiently resolved by HPLC. For the validity of FAB-MS quantification of compounds in mixtures see also: A.E. Manzi, A. Dell, P. Azadi, and A. Varki J. Biol. Chem. 265 1990 8094
    • (1990) J. Biol. Chem. , vol.265 , pp. 8094
    • Manzi, A.E.1    Dell, A.2    Azadi, P.3    Varki, A.4
  • 24
    • 85030812128 scopus 로고    scopus 로고
    • note
    • The DCL products 4aacf exist as three possible isomers (regioisomers and enantiomeric stereoisomers) and 4ccg as two possible regioisomers. From the NMR data obtained it is currently not possible to distinguish and unambigiously assign the structure of the major reaction products


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.