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note
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In the iron-catalyzed Grignard cross-coupling, Fe(I), Fe(II), and Fe(-II) species are proposed as catalytically active species: see ref 12c and references therein.
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note
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Generation of ethylene was confirmed by trapping the evolved gas with bromine, which gave 1,2-dibromoethane. See also ref 15.
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33
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0037205911
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note
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Low yield was also observed in the homo-coupling of phenyllithium giving biphenyl (38% yield, ether reflux for 1 h).
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