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note
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The details of synthesis of ligand 1 will be reported elsewhere.
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note
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1 = 0.0622; wR2 = 0.1191 (I > 2σ(I)); Data/restraints/ parameter = 2230/0/ 170. CCDC-243911-243912 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB21EZ, UK.; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
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