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Volumn 5, Issue 1, 2005, Pages 337-340

Cocrystal of an ionic liquid with organic molecules as a mimic of ionic liquid solution

Author keywords

[No Author keywords available]

Indexed keywords

1 METHYL 3 N BUTYLIMIDAZOLIUM BROMIDE; BROMINE DERIVATIVE; ORGANIC COMPOUND; UNCLASSIFIED DRUG;

EID: 12844271223     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg030086i     Document Type: Article
Times cited : (26)

References (33)
  • 5
    • 0000544358 scopus 로고    scopus 로고
    • (e) Wasserscheid, P.; Keim, W. Angew. Chem. 2000, 112, 3926; Wasserscheid, P.; Keim, W. Angew. Chem., Int. Ed. 2000, 39, 3772.
    • (2000) Angew. Chem. , vol.112 , pp. 3926
    • Wasserscheid, P.1    Keim, W.2
  • 25
    • 12844277611 scopus 로고    scopus 로고
    • note
    • 2, J(HH) = 7.2 Hz), 8.28 (s, 1 H, H5 (Im)), 8.38 (s, 1 H, H4 (Im)), 10.02 (s, 1 H, H2 (Im)). Procedure for the preparation of cocrystal of PD 1: 1-methyl-3-n-butyl imidazolium bromide (0.30 g, 0.0014 mol) and 1,4-phenylenediamine (0.15 g, 0.0014 mol) were put into the three-necked flask. The mixture was heated to 140°C under inert flow with stirring. After complete dilution of components, the reaction mass was cooled to room temperature forming brown crystals. DSC measurements were carried out using Mettler 822 with heat grade equal to 10°C/min.
  • 33
    • 12844283560 scopus 로고    scopus 로고
    • note
    • 2 = 0.1000 and GOF = 1.028 for all independent reflections (R1 = 0.0487 was calculated against F for 2506 observed reflections with I > 2σ(I)). All calculations were performed using SHELXTL PLUS 5.1.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.