Synthesis and reactivity of novel alkali metal stannides

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Volumn 59, Issue 11-12, 2004, Pages 1462-1470

  Schollmeier, Thorsten ^b   Englich, Ulrich ^c   Fischer, Roland ^a   Prass, Ingo ^b   Ruhlandt, Karin ^c   Schürmann, Markus ^b   Uhlig, Frank ^a  

^a GRAZ UNIVERSITY OF TECHNOLOGY   (Austria)

^b TU DORTMUND UNIVERSITY   (Germany)

^c SYRACUSE UNIVERSITY   (United States)

Author keywords

Alkali Metal Stannides; Preparation; Reactivity, 119Sn and 29Si NMR Spectroscopy; Structure Elucidation

Indexed keywords

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POTASSIUM COMPOUNDS; SILICON;

29SI NMR; BUTYLTIN COMPOUNDS; MULTINUCLEAR NMR SPECTROSCOPY; POTASSIUM HYDRIDES; PREPARATION; SIDE PRODUCTS; STRUCTURE ELUCIDATION; SYNTHESIS AND CHARACTERIZATIONS;

X RAY CRYSTALLOGRAPHY;

ALKALI METAL; HYDROGEN; POTASSIUM HYDRIDE; TIN DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CELL NUCLEUS; CHEMICAL REACTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SUBSTITUTION REACTION; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 12444333504     PISSN: 09320776     EISSN: None     Source Type: Journal    
DOI: 10.1515/znb-2004-11-1215     Document Type: Article

References (34)

1. P. Riviere, A. Castel, M. Riviere-Baudet, Alkaline and alkaline earth metal-14 compounds: Preparation, spectroscopy and reactivity, in: Z. Rappoport (ed.): The chemistry of organo-germanium, tin, and lead compounds (Chemistry of functional groups), pp. 653, John Wiley & Sons, Chichester (2002).
2. J. P. Quintard, M. Pereyre, Reviews on Silicon, Germanium, Tin and Lead Compounds 4 (3), 151 (1980).
3. Y. Matsuhashi, N. Tokitoh, R. Okazaki, M. Goto, S. Nagase, Organometallics 12, 1351 (1993).
4. M.-F. Connil, B. Jousseaume, M. Pereyre, Organometallics 15, 4469 (1996).
5. S. P. Mallela, R. A. Geanangel, Inorg. Chem. 32, 5623 (1993).
6. T. Lobreyer, W. Sundermeyer, H. Oberhammer, Chem. Ber. 127, 2111 (1994).
7. F. Uhlig, C. Kayser, R. Klassen, U. Hermann, L. Brecker, M. Schürmann, K. Ruhlandt-Senge, U. Englich, Z. Naturforsch. 54b, 278 (1999).
8. P. Bleckmann, U. Englich, U. Hermann, I. Prass, K. Ruhlandt-Senge, M. Schürmann, C. Schwittek, F. Uhlig, Z. Naturforsch. 54b, 1188 (1999).
9. U. Englich, I. Prass, K. Ruhlandt-Senge, T. Schollmeier, F. Uhlig, Monatsh. Chem. 133, 931 (2002).
10. M. Schürmann, T. Schollmeier, F. Uhlig, unpublished results.
11. U. Hermann, G. Reeske, M. Schürmann, F. Uhlig, Z. Anorg. Allg. Chem. 627, 453 (2001).
12. M. Schürmann, I. Prass, F. Uhlig, Organometallics 19, 2546 (2000).
13. U. Englich, U. Hermann, I. Prass, T. Schollmeier, K. Ruhlandt Senge, F. Uhlig, J. Organomet. Chem. 646, 271 (2001).
14. G. Wittig, F. J. Meier, G. Lange, Liebigs Ann. Chem. 571, 167 (1951).
15. W. C. Still, J. Am. Chem. Soc. 100, 1481 (1978).
16. R. J. P. Corriu, C. Guerin, J. Organomet. Chem. 197, C19 (1980).
17. S. Sharma, A. C. Oelschlaeger, J. Org. Chem. 54, 5064 (1989).
18. D. Reed, D. Stalke, D. S. Wright, Angew. Chem. 103, 1539 (1991).
19. W. Reimann, H. G. Kuivila, D. Farah, T. Apoussidis, Organometallics 6, 557 (1987).
20. D. Farah, T. J. Carol, H. G. Kuivila, Organometallics, 4, 662 (1985).
21. D. Reed, D. Stalke, D. S. Wright, Angew. Chem. 103, 1539 (1991).
22. P. B. Hitchcock, M. F. Lappert, G. A. Lawless, B. Royo, J. Chem. Soc., Chem. Commun. 554 (1993).
23. U. Englich, K. Ruhlandt-Senge, F. Uhlig, J. Organomet. Chem. 613, 139 (2000).
24. R. Fischer, J. Baumgartner, C. Marschner, F. Uhlig, in preparation.
25. K. Hassler, unpublished results.
26. G. M. Sheldrick, Acta Crystallogr. A46, 467 (1990).
27. G. M. Sheldrick, SHELXL-97, University of Göttingen, Germany (1997).
28. S. Chadwick, U. Englich, B. Noll, K. Ruhlandt-Senge, Inorg. Chem. 37, 4718 (1998).
29. H. Hope, Progr. Inorg. Chem. 41, 1 (1994).
30. G. M. Sheldrick, SADABS, Program for Absorption Correction Using Area Detector Data; University of Göttingen, Germany (1996).
31. Siemens SHELXTL-Plus, Siemens: Madison, Wisconsin (1996).
32. G. M. Sheldrick, SHELXL-93, University of Göttingen, Germany (1993).
33. International Tables for Crystallography, Vol. C, Kluwer Academic Publishers, Dordrecht (1992).
34. G. M. Sheldrick, SHELXTL, Release 5.1 Software Reference Manual, Bruker AXS Inc., Madison, Wisconsin (1997).