Gradient ion-pair chromatographic method for the determination of iron N,N′-ethylenediamine-di-(2-hydroxy-5-sulfophenylacetate) by high performance liquid chromatography-atmospheric pressure ionization electrospray mass spectrometry

Journal of Chromatography A

Volumn 1064, Issue 1, 2005, Pages 67-74

  García Marco, Sonia ^a   Cremonini, Mauro A ^b   Esteban, Pedro ^c   Yunta, Felipe ^a   Hernández Apaolaza, Lourdes ^a   Placucci, Giuseppe ^b   Lucena, Juan J ^a  

^a UNIVERSIDAD AUTÓNOMA DE MADRID   (Spain)

^b UNIVERSITY OF BOLOGNA   (Italy)

^c SA Dabeer   (Spain)

Author keywords

Chelated iron; EDDHSA Fe3+; Fertilizers; HPLC APIES MS; N,N Ethylenediamine di (2 hydroxy 5 sulfophenylacetic acid)

Indexed keywords

AMINES; CARBOXYLIC ACIDS; CONDENSATION; FERTILIZERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIZATION; IRON COMPOUNDS; MASS SPECTROMETRY;

CHROMATOGRAPHIC PEAKS; ELECTROSPRAY MASS SPECTROMETRY; ION-PAIR CHROMATOGRAPHIC METHOD; IRON CHELATION;

CHROMATOGRAPHIC ANALYSIS;

ACETONITRILE; ETHYLENEDIAMINE DERIVATIVE; FERTILIZER; HYDROXIDE; IRON CHELATE; MONOMER; TETRABUTYLAMMONIUM;

ACIDITY; AQUEOUS SOLUTION; CONFERENCE PAPER; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INSTRUMENTATION; ION PAIR CHROMATOGRAPHY; IRON CHELATION; IRON DEFICIENCY; MASS SPECTROMETRY; MOLECULE; PARAMETER; POLYMERIZATION; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS;

ATMOSPHERIC PRESSURE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HYDROGEN-ION CONCENTRATION; PHENYLACETATES; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

CARBOXYLIC ACIDS; CHELATES; CHROMATOGRAPHY; FERTILIZERS; IONIZATION; IRON COMPOUNDS; MASS SPECTROSCOPY; POLYAMINES;

EID: 12344275774     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2004.12.028     Document Type: Conference Paper

References (30)

1. Y. Chen, and P. Barak Adv. Agron. 35 1982 217
2. W.L. Lindsay Chemical Equilibria in Soils 1979 Wiley New York
3. S. Ahrland, A. Dahlgren, and I. Persson Acta Agric. Scand. 40 1990 101
4. G.C. Liu, Y.M. Wang, T.S. Jaw, H.M. Chen, and R.S. Sheu J. Formosan Med. Assoc. 92 4 1993 359
5. A.E. Martell, R.J. Motekaitis, Y. Sun, R. Ma, M.J. Welch, and T. Pjeau Inorg. Chim. Acta 91 1999 238
6. M. Dexter, Preparation of phenolic ethylenediaminepolycarboxylic acids. US Patent 2,824,128 (1958).
7. A. Álvarez-Fernández, Quality and Efficiency of Iron Chelates (FeEDDHA, FeEDDHMA, FeEDDHSA y FeEDDCHA) as Fertilizers (In Spanish). Ph. Dissertation, University Autónoma of Madrid, Madrid, 2000.
8. H.E. Petree, J.W. Stutts, Iron complexes of ethylenebis(α-imino-2- hydroxyarylacetic acids). US Patent 3,903,119 (1975).
9. A. Badrinas, P. Esteban, Procedure for obtaining a chelate of iron of high solubility. Spain Patent ES2044777 (1994).
10. H.E. Petree, J.W. Stutts, Treatment of iron deficiencies in plants with iron complexes of ethylene-bis-(-α-imino-2-hydroxyaril acetic acids). US Patent 3,981,712 (1976).
11. H.E. Petree, H.L. Myatt, A.M. Jelenevsky, Preparation of phenolic ethylenediaminepolycarboxylic acids). US Patent 4,130,582 (1978).
12. J.A.L. Jullien, A. Aymard, Preparation of ethylenediaminebis(o- hydroxyphenylacetic acids) as chelating agents. European Patent Application EP0331556A2 (1989).
13. M. Knell, H. Kroll, Ethylenediamine derivatives. US Patent 300584819611024 (1961).
14. F. Yunta, S. García-Marco, J.J. Lucena, M. Gómez-Gallego, R. Alcázar, and M.A. Sierra Inorg. Chem. 42 2003 5412
15. A. Álvarez-Fernández, M.A. Cremonini, M.A. Sierra, G. Placucci, and J.J. Lucena J. Agric. Food Chem. 50 2 2002 284
16. A. Álvarez-Fernández, M.A. Sierra, and J.J. Lucena Plant Soil 241 2002 129
17. D.G. Hill-Cottingham J. Chromatogr. 8 1962 261
18. M.G. Patch, K.S. Simlo, and C.J. Carrano J. Inorg. Chem. 21 1982 2972
19. R. Boxema Pflanzenernaehr. Bodenkd. 142 1979 824
20. J. Bannochie, and A.E. Martell J. Am. Chem. Soc. 111 1989 4735
21. P. Barak, and Y. Chen Soil Sci. Soc. Am. J. 51 1987 893
22. M. Deacon, M.R. Smyth, and L.G.M. Tuinstra J. Chromatogr. A 659 1994 349
23. J.J. Lucena, P. Barak, and L. Hernández-Apaolaza J. Chromatogr. A 727 1996 253
24. L. Hernández-Apaolaza, P. Barak, and J.J. Lucena J. Chromatogr. A 789 1997 453
25. L. Hernández-Apaolaza, A. Álvarez-Fernández, and J.J. Lucena J. Plant Nutr. 23 11-12 2000 2035
26. ASTM. Standard Specification for Reagente Water, Annual Book of ASTM Standards, 1995, 11.01.
27. D.G. Hill-Cottingham Nature 175 1955 347
28. C.T. Hung, and R.B. Taylor J. Chromatogr. 202 1980 333
29. H.H. Jaffe, and M. Orchin Theory and Applications of Ultraviolet Spectroscopy 1962 Wiley New York
30. R.G. Cantera, A.M. Zamarreño, and J.M. García-Mina J. Agric. Food Chem. 50 2002 7609