Thermodynamic study of N-trifluoroacetyl-O-alkyl nipecotic acid ester enantiomers on diluted permethylated β-cyclodextrin stationary phase

Journal of Chromatography A

Volumn 1064, Issue 2, 2005, Pages 193-204

  McGachy, Neil T ^a   Grinberg, Nelu ^b   Variankaval, Narayan ^a  

^a MERCK RESEARCH LABORATORIES   (United States)

^b BOEHRINGER INGELHEIM PHARMACEUTICALS INC   (United States)

Author keywords

Gas chromatography; Nipecotic acid; Permethylated cyclodextrin; Retention increment method; Thermodynamic parameters

Indexed keywords

CARBOXYLIC ACIDS; COMPLEXATION; ENTHALPY; ESTERS; MOLECULAR STRUCTURE; MOLECULAR WEIGHT; STEREOCHEMISTRY;

ALKYL GROUPS; ENANTIOMERS; ENANTIOSELECTIVE INTERACTIONS; RETENTION INCREMENT METHODS;

MOLECULAR ORIENTATION;

BETA CYCLODEXTRIN DERIVATIVE; ESTER DERIVATIVE; NIPECOTIC ACID DERIVATIVE;

ANALYTICAL EQUIPMENT; ARTICLE; DIASTEREOISOMER; DILUTION; ENANTIOMER; ENANTIOSELECTIVITY; ENTHALPY; ENTROPY; MOLECULAR DYNAMICS; MOLECULAR INTERACTION; MOLECULAR WEIGHT; PRIORITY JOURNAL; THERMODYNAMICS;

BETA-CYCLODEXTRINS; INDICATORS AND REAGENTS; MODELS, MOLECULAR; NIPECOTIC ACIDS; STEREOISOMERISM; TEMPERATURE; THERMODYNAMICS;

EID: 12344274415     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2004.12.013     Document Type: Article

References (26)

1. V. Schurig J. Chromatogr. A 906 2001 275
2. C. Bicchi, A. D'Amato, and P. Rubiolo J. Chromatogr. A 843 1999 99
3. W.A. König Gas Chromatographic Enantiomer Separation with Modified Cyclodextrins 1992 Hüthig Heidelberg, Germany
4. A. Dietrich, B. Maas, and A. Mosandl J. High Resolut. Chromatogr. 18 1995 152
5. Z. Juvancz, G. Alexander, and J. Szejtli J. High Resolut. Chromatogr., Chromtogr. Commun. 10 1987 105
6. V. Schurig, and H.P. Nowotny J. Chromatogr. 441 1988 155
7. J. Mraz, L. Feltl, and E. Smolkova-Keulemansova J. Chromatogr. 286 1984 17
8. J. Krupcik, E. Benicka, P. Majek, I. Skacani, and P. Sandra J. Chromatogr. A 665 1994 175
9. I. Spanik, P. Oswald, J. Krupcik, E. Benicka, P. Sandra, and D. Armstrong J. Sep. Sci. 25 2002 45
10. U.J. Meierhenrich, M. Nguyen, B. Barbier, A. Brack, and W. Thiemann Chirality 15 2003 13
11. E. Benicka, J. Krupcik, I. Spanik, J. Hrouzek, and P. Sandra J. Microcolumn Sep. 8 1996 57
12. M. Jung, D. Schmalzing, and V. Schurig J. Chromatogr. 552 1991 43
13. B. Furniss, A. Hannaford, P. Smith, and A. Tatchell Vogel's Textbook of Practical Organic Chemistry 1999 Longman Group UK
14. W. König, and I. Benecke J. Chromatogr. 269 1983 19
15. I. Spanik, J. Krupcik, and V. Schurig J. Chromatogr. A 843 1999 123
16. V. Schurig, and M. Juza J. Chromatogr. A 757 1997 119
17. M. Rekharsky, and Y. Inoue Chem. Rev. 98 1998 1875
18. M. Rekharsky, M. Mayhew, R. Goldberg, P. Ross, Y. Yamashoji, and Y. Inoue J. Phys. Chem. B 101 1997 87
19. C. Bicchi, C. Brunelli, G. Cravotto, P. Rubiolo, M. Galli, and F. Mendicuti J. Sep. Sci. 26 2003 761
20. M. Schneider, and K. Ballschmiter J. Chromatogr. A 852 1999 525
21. V. Schurig, and R. Schmidt J. Chromatogr. A 1000 2003 311
22. R.R. Krug, W.G. Hunter, and R.A. Grieger J. Phys. Chem. 80 1976 2335
23. R.R. Krug, W.G. Hunter, and R.A. Grieger J. Phys. Chem. 80 1976 2341
24. W. Melander, D.E. Campbell, and C. Horvath J. Chromatogr. 158 1978 215
25. A. Berthod, W. Li, and D.W. Armstrong Anal. Chem. 64 1992 873
26. K. Lipkowitz, R. Coner, M. Peterson, A. Morreale, and J. Shackelford J. Org. Chem. 63 1998 732