메뉴 건너뛰기




Volumn 46, Issue 5, 2005, Pages 755-758

A facile access to chalcogen and dichalcogen bearing dialkylamines and diols

Author keywords

Amines; Diols; Selenium; Synthesis; Tellurium

Indexed keywords

ALCOHOL DERIVATIVE; ALIPHATIC AMINE; CHALCOGEN; DIAMINE DERIVATIVE; DICHALCOGEN; INORGANIC COMPOUND; SELENIUM; TELLURIUM; UNCLASSIFIED DRUG;

EID: 11844269887     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2004.12.035     Document Type: Article
Times cited : (31)

References (29)
  • 12
  • 13
    • 11844259798 scopus 로고    scopus 로고
    • note
    • + or PhSeH and their utility in organic transformations
  • 16
    • 11844251663 scopus 로고    scopus 로고
    • note
    • These two articles cover the stereoselective synthesis of oxygenated heterocyclic rings from mixtures of hydroxy selenides
  • 19
    • 0342947407 scopus 로고
    • 2OH after distillation. Following this procedure, we observed the formation of both 1 and 9 ; extraction and purification of the product from the resulting mixture proved to be a long and tedious procedure. During distillation of the final product, extensive decomposition was observed and the product, in our hands, was obtained in a yield of 25-32%
    • (1977) Acta Chem. Scand. Ser. B , vol.31 , pp. 1-6
    • Lingren, B.1
  • 20
    • 11844282493 scopus 로고
    • I.K. Sang, and C.P. Spears Synthesis 1988 133 135 this method involves reaction of 2-bromoethanol with potassium selenocyanate in boiling acetone to give 2-hydroxyethylselenocyanate in 80% yield. The selenocyanate was converted in situ in the presence of sodium borohydride to the corresponding selenolate anions which react with electrophilic substrate
    • (1988) Synthesis , pp. 133-135
    • Sang, I.K.1    Spears, C.P.2
  • 21
    • 0242270866 scopus 로고    scopus 로고
    • T.G. Back, and Z. Moussa J. Am. Chem. Soc. 125 2003 13455 13460 this article deals with a series of aliphatic diselenides and selenides containing coordinating substituents which were tested for glutathione peroxidase (GPx)-like catalytic activity in a model system in which the reduction of tert-butyl hydroperoxide with benzyl thiol to afford dibenzyl disulfide and tert-butyl alcohol was performed under standard conditions. In particular, allyl 3-hydroxypropyl selenide rapidly generated 1,2-oxaselenolane Se-oxide in situ by a series of oxidation and [2,3]sigmatropic rearrangement steps
    • (2003) J. Am. Chem. Soc. , vol.125 , pp. 13455-13460
    • Back, T.G.1    Moussa, Z.2
  • 26
    • 11844279439 scopus 로고
    • Academic Press Limited London N.
    • Tellurium in Organic Synthesis; N. Petragnani 1994 Academic Press Limited London John Wiley and Sons, New York, 1973
    • (1994)
    • Petragnani1
  • 27
    • 11844281266 scopus 로고    scopus 로고
    • note
    • 2)
  • 28
    • 11844282496 scopus 로고    scopus 로고
    • note
    • 13C (75 MHz), δ 44.29 (N-C), 36.27 (C-C), 9.15 (Te-C)
  • 29
    • 11844252951 scopus 로고    scopus 로고
    • note
    • 2).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.