Combined in situ 29Si NMR and small-angle X-ray scattering study of precursors in MFI zeolite formation from silicic acid in TPAOH solutions

Physical Chemistry Chemical Physics

Volumn 5, Issue 16, 2003, Pages 3518-3524

  Houssin, Christophe J Y ^a   Kirschhock, Christine E A ^b   Magusin, Pieter C M M ^a   Mojet, Barbara L ^a   Grobet, Piet J ^b   Jacobs, Pierre A ^b   Martens, Johan A ^b   Van Santen, Rutger A ^a  

^a EINDHOVEN UNIVERSITY OF TECHNOLOGY   (Netherlands)

^b UNIVERSITY OF LEUVEN   (Belgium)

Author keywords

[No Author keywords available]

Indexed keywords

OLIGOMER; SILICATE; SILICIC ACID; SILICON; SODIUM; TETRAPROPYLAMMONIUM; ZEOLITE;

ARTICLE; COLLOID; CRYSTALLIZATION; HEATING; NUCLEAR MAGNETIC RESONANCE; POLYMERIZATION; POWDER; ROOM TEMPERATURE; SYNCHROTRON RADIATION; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 11344284034     PISSN: 14639076     EISSN: None     Source Type: Journal    
DOI: 10.1039/b306988p     Document Type: Article

References (48)

1. R. Szostak, Molecular sieves, Blackie Academic & Professional, Glasgow-London, 1998.
2. P. B. Venuto, Microporous Mater., 1994, 2, 297.
3. H. Van Bekkum, E. M. Flanigen, P. A. Jacobs and J. C. Jansen, Introduction to zeolite science and practice, Studies in Surface Science and Catalysis Series, Elsevier, Amsterdam, 2nd edn., 2001.
4. C. Baerlocher, W. M. Meier and D. H. Olson, Atlas of zeolite framework type, Elsevier, Amsterdam, 5th revised edn., 2001.
5. B. M. Lok, T. R. Cannan and C. A. Messina, Zeolites, 1983, 3, 282.
6. S. Mintova, N. H. Olson, J. Senker and T. Bein, Angew. Chem., Int. Ed., 2002, 41, 2558.
7. H. Gies and B. Marler, Zeolites, 1992, 12, 42.
8. M. E. Davis and S. I. Zones, Synthesis of Porous Materials: zeolites, clays and nanostructures, Marcel Dekker, New York, 1997, p. 1.
9. S. L. Burkett and M. E. Davis, J. Phys. Chem., 1994, 98, 4467.
10. R. Gougeon, L. Delmotte, D. Le Nouen and Z. Gabelica, Microporous Mesoporous Mater., 1998, 26, 43.
11. J. N. Watson, L. E. Iton, R. I. Keir, J. C. Thomas, T. L. Dowling and J. W. White, J. Phys. Chem. B, 1997, 101, 10094.
12. (a) R. K. Harris and C. T. G. Knight, J. Mol. Struct., 1982, 78, 273;
13. (b) R. K. Harris and C. T. G. Knight, J. Chem. Soc., Faraday Trans. 2., 1983, 79, 1525;
14. (c) R. K. Harris and C. T. G. Knight, J. Chem. Soc., Faraday Trans. 2., 1983, 79, 1539;
15. (d) C. T. G. Knight, J. Chem. Soc., Dalton Trans., 1988, 1457.
16. (a) D. Hoebbel, G. Garzo, G. Engelhardt, R. Ebert, E. T. Lippmaa and M. Z. Alla, Anorg. Allg. Chem., 1980, 465, 15;
17. (b) D. Hoebbel, G. Garzo, G. Engelhardt and A. Z. Vargha, Anorg. Allg. Chem., 1982, 494, 31;
18. (c) D. Hoebbel, A. Vargha, G. Engelhardt and K. Z. Usjszaszy, Anorg. Allg. Chem., 1984, 509, 85;
19. (d) G. Engethardt and D. Michel, High-Resolution Solid-State NMR of Silicates and Zeolites, John Wiley & Sons, New York, 1987.
20. (a) S. D. Kinrade, C. T. G. Knight, D. L. Pole and R. T. Syvitski, Inorg. Chem., 1998, 37, 4272;
21. (b) S. D. Kinrade, C. T. G. Knight, D. L. Pole and R. T. Syvitski, Inorg. Chem., 1998, 37, 4278.
22. (a) R. K. Harris, J. Parkinson and A. J. Samadi-Maybodi, J. Chem. Soc., Dalton Trans., 1997, 2553;
23. (b) S. D. Kinrade, J. C. H. Donovan, A. S. Schach and C. T. G. Knight, J. Chem. Soc., Dalton Trans., 2002, 1250.
24. P. A. Jacobs and J. A. Martens, Synthesis of high-silica alumino-silicates zeolites, Studies in Surface Science and Catalysis Series, Elsevier Science, New York, 1987, vol. 33.
25. C. E. A. Kirschhock, R. Ravishankar, F. Verspeurt, P. J. Grobet, P. A. Jacobs and J. A. Martens, J. Phys. Chem. B, 1999, 103, 4965.
26. C. E. A. Kirschhock, S. P. B. Kremer, P. J. Grobet, P. A. Jacobs and J. A. Martens, J. Phys. Chem. B, 2002, 106, 4897.
27. C. E. A. Kirschhock, V. Buschmann, S. Kremer, R. Ravishankar, C. J. Y. Houssin, B. L. Mojet, P. J. Grobet, R. A. van Santen, P. A. Jacobs and J. A. Martens, Angew. Chem., Int. Ed., 2001, 40, 2637.
28. C. E. A. Kirschhock, R. Ravishankar, P. A. Jacobs and J. A. Martens, J. Phys. Chem. B, 1999, 103, 11021.
29. C. J. Y. Houssin, B. L. Mojet, C. E. A. Kirschhock, V. Buschmann, P. A. Jacobs, J. A. Martens and R. A. van Santen, Zeolites and Mesoporous Materials at the Dawn of the 21st Century, Stud. Surf. Sci. Catal.. 2001, 135, 135.
30. P.-P. E. A. De Moor, T. P. M. Beelen, B. U. Komanshek, O. Diat and R. A. van Santen, J. Phys. Chem. B, 1997, 101, 11077.
31. P.-P. E. A. De Moor, T. P. M. Beelen, B. U. Komanschek, L. W. Beck, P. Wagner, M. E. Davis and R. A. van Santen, Chem.-Eur. J., 1999, 5, 2083.
32. P.-P. E. A. De Moor, T. P. M. Beelen, R. A. van Santen, K. Tsuji and M. E. Davis, Chem. Mater., 1999, 11, 36.
33. P.-P. E. A. De Moor, T. P. M. Beelen and R. A. van Santen, J. Phys. Chem. B, 1999, 103, 1639.
34. P.-P. E. A. De Moor, T. P. M. Beelen, R. A. van Santen, L. W. Beck and M. E. Davis, J. Phys. Chem. B, 2000, 104, 7600.
35. J. P. Verduijn, Exxon Patent, PCT/EP92/02386, 1992.
36. T. Narayanan, O. Diat and P. Bösecke, Nucl. Instrum. Methods Phys. Res., Sect. A, 2001, 467-468, 1005.
37. U. Bonse and M. Hart, in Small-angle X-ray scattering, Gordon and Breach, New York, 1967, p. 121.
38. O. Diat, P. Bösecke, J. Lambard and P.-P. E. A. De Moor, J. Appl. Crystallogr., 1997, 30, 862.
39. R. K. Iler, The chemistry of silica, John Wiley and Sons, New York, 1979.
40. P. W. J. G. Wijnen, T. P. M. Beelen, J. W. de Haan, C. P. J. Rummens, L. J. M. van de Ven and R. A. van Santen, J. Non-Cryst. Solids, 1989, 109, 85.
41. G. Engelhardt, H. Jancke, M. Mage, T. Pehk and E. Lippma, J. Organomet. Chem., 1971, 28, 293.
42. R. F. Mortlock, A. T. Bell and C. J. Radke, J. Phys. Chem., 1991, 95, 372.
43. C. T. G. Knight and S. D. Kinrade, J. Phys. Chem. B, 2002, 106, 3329.
44. C. T. G. Knight and S. D. Kinrade, Inorg. Chem., 1988, 27, 4253.
45. G. Boxhoorn, O. Sudmeijer and P. H. G. van Kasteren, J. Chem. Soc., Chem. Commun., 1983, 1426.
46. B. J. Schoeman and O. Regev, Zeolites, 1996, 17, 447.
47. B. J. Schoeman, Zeolites, 1997, 18, 97.
48. J. J. Keijsper and M. F. Post, in Zeolite synthesis, ed. M. L. Ocelli and H. E. Robson, ACS Symposium Series 398, American Chemical Society, Washington, DC, 1988, p. 28.