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5N: C, 55.16; H, 8.87; N, 5.36. Found: C, 55.14; H, 9.01; N, 5.31. For characterization of 1: Ref. 2a For characterization of 2, 6 and 7 see Ref. 10e and citations therein
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38
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11144333649
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note
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1H NMR). A similar product distribution was observed in Refs. a and b
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39
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0000266497
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Subjection of methyl cyclohexanecarboxylate to the reaction conditions did not result in the formation of 9 but instead returned unreacted ester. For further discussion see Refs. a and b. For related reactions see: B.D. Mookherjee, R.W. Trenkle, and R. Patel J. Org. Chem. 36 1971 3266 3270
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41
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0030829196
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2O: C, 55.50; H, 9.20; N, 4.98. Found C, 55.71; H, 8.95; N, 4.92. For characterization of 11, see Ref. 2a. For characterization of 12, see: H. Yamamoto, M. Tsuda, S. Sakaguchi, and Y. Ishii J. Org. Chem. 62 1997 7174 7177
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0026008522
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For characterization of 14, see: M. Boni, L. Forti, F. Ghelfi, and U.M. Pagoni Tetrahedron 50 1994 7897 7902
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