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33646668740
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note
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6: C, 75.86; H, 5.25; N, 2.21. Found: C, 75.93; H, 5.71; N, 2.43
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27
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33646642289
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note
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2 by a full-matrix least-squares method. Anisotropic displacement parameters were included for all non-hydrogen atoms. All the calculations were carried out with Siemens SHELXTL PLUS program. Crystallographic data for the structural analysis have been deposited with the Cambridge Crystallographic Data Center CCDC Nos. 248435 and 248436
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28
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0031576308
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S.Y. Desjardins, K.J. Cavell, J.L. Hoare, B.W. Skelton, A.N. Sobolev, A.H. White, and W. Keim J. Organomet. Chem. 544 1997 163
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Desjardins, S.Y.1
Cavell, K.J.2
Hoare, J.L.3
Skelton, B.W.4
Sobolev, A.N.5
White, A.H.6
Keim, W.7
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30
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33646655597
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note
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Determined using a PL GPC-220 gel permeation chromatograph at 150°C with narrow standard calibration and equipped with three PL gel columns (sets of PL gel 10 μm Mixed-B LS), and 1,2,4-trichlorobenzene was used as solvent at a flow rate of 1.00 ml/min
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31
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33646656697
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note
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13C NMR (o-dichlorobenzene-d4): δ = 29-52 ppm (m, maxima at 31.1, 38.1, 47.1)
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