Application of HMQC spectroscopy to the observation of the metal resonance in polymetallic compounds: The effect of multiple-metal spin transitions

Magnetic Resonance in Chemistry

Volumn 42, Issue 9, 2004, Pages 769-775

  Heaton, B T ^a   Iggo, J A ^a   Podkorytov, I S ^b   Tunik, S P ^c  

^a UNIVERSITY OF LIVERPOOL   (United Kingdom)

^b Lebedev Research Institute of Synthetic Rubber   (Russian Federation)

^c ST PETERSBURG STATE UNIVERSITY   (Russian Federation)

Author keywords

103Rh NMR; 13C NMR; 31P NMR; HMQC; Metal carbonyl clusters; Multiple spin transitions; NMR

Indexed keywords

CARBONYLATION; CARBOXYLATION; CHEMICAL SHIFT; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

103RH NMR; 13C NMR; 31P-NMR; CROSS PEAKS; HMQC; METAL-CARBONYL CLUSTERS; MULTIPLE METALS; MULTIPLE SPIN TRANSITION; SPECTRA'S; SPIN TRANSITION;

RHODIUM COMPOUNDS;

RHODIUM DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL ANALYSIS; CORRELATION ANALYSIS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE;

EID: 10944236939     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1428     Document Type: Article

References (23)

1. von Philipsborn W. Chem. Soc. Rev. 1999; 28: 95.
2. Donkervoort JG, Buhl M, Ernsting JM, Elsevier CJ. Eur. J. Inorg. Chem. 1999; 27.
3. Carlton L. Inorg. Chem. 2000; 39: 4510.
4. Berners-Price SJ, Bowen RJ, Harvey PJ, Healy PC, Koutsantonis GA. J. Chem. Soc., Dalton Trans. 1998; 1743.
5. Nanz D, von Philipsborn W. J. Magn. Reson. 1991; 92: 560.
6. Grachova EV, Heaton BT, Iggo JA, Podkorytov IS, Smawfield DJ, Tunik SP, Whyman R. J. Chem. Soc., Dalton Trans. 2001; 3303.
7. Sabounchei JSZ, Heaton BT, Iggo JA, Jacob C, Podkorytov IS. J. Cluster Sci. 2001; 12: 339.
8. Heaton BT, Iggo JA, Podkorytov IS, Smawfield DJ, Tunik SP, Whyman R. J. Chem. Soc., Dalton Trans. 1999; 1917.
9. Dolgushin FM, Grachova EV, Heaton BT, Iggo JA, Koshevoy IO, Podkorytov IS, Smawfield DJ, Tunik SP, Whyman R, Yanovskii AI. J. Chem. Soc., Dalton Trans. 1999; 1609.
10. Farrar DH, Grachova EV, Haukka M, Heaton BT, Iggo JA, Pakkanen TA, Podkorytov IS, Tunik SP. Inorg. Chim. Acta 2003; 354: 11.
11. Ruegger H, Moskau D. Magn. Reson. Chem. 1991; 29: S11.
12. Magiera D, Baumann W, Podkorytov IS, Omelanczuk J, Duddeck H. Eur. J. Inorg. Chem. 2002; 3253.
13. Tunik SP, Podkorytov IS, Heaton BT, Iggo JA, Sampanthar J. J. Organomet. Chem. 1998; 550: 221.
14. Farrar DH, Grachova EV, Lough A, Patirana C, Poe AJ, Tunik SP. J. Chem. Soc., Dalton Trans. 2001; 2015.
15. Ernst RR, Bodenhausen G, Wokaun A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Oxford University Press: Oxford, 1987.
16. Sorensen OW, Eich GW, Levitt MH, Bodenhausen G, Ernst RR. Prog. Nucl. Magn. Reson. Spectrosc. 1983; 16: 163.
17. Heaton BT, Iggo JA, Podkorytov IS, Smawfield DJ, Tunik SP, Whyman R. In Metal Clusters in Chemistry, vol. 3, Braunstein P, Oro L, Raithby PR, (eds). Wiley-VCH: Weinheim, 1999; 960.
18. Maginn SJ. Acta Crystallogr., Sect. C 1990; 46: 576.
19. Heaton BT, Strona L, Della Pergola R, Garlaschelli L, Sartorelli U, Sadler IH. J., Chem. Soc., Dalton Trans. 1983; 173, and references cited therein.
20. Heaton BT, Longhetti L, Mingos DMP, Briant CE, Minshall PC, Theobald BRC, Garlaschelli L, Sartorelli U. J. Organomet. Chem. 1981; 213: 333.
21. Albano VG, Braga D, Grepioni F. Acta Crystallogr., Sect. B 1989; 45: 60.
22. Heaton BT, Iggo JA, Longoni G, Mulley S. J. Chem. Soc., Dalton Trans. 1995; 1985.
23. Martinengo S, Strumolo D, Chini P. Inorg. Synth. 1980; 20: 212.