One-pot synthesis and self-assembly of double stranded helical metal complexes

Inorganic Chemistry Communications

Volumn 7, Issue 2, 2004, Pages 249-252

  Wu, Zhikun ^a   Yang, Guoqiang ^a   Chen, Qingqi ^b   Liu, Jingang ^a   Yang, Shiyong ^a   Ma, Jin Shi ^a  

^a INSTITUTE OF CHEMISTRY   (China)

^b BIOMARIN PHARMACEUTICAL INC   (United States)

Author keywords

Helicates; One pot synthesis; Schiff base; Self assembly; Supramolecules

Indexed keywords

METAL COMPLEX; ZINC COMPLEX;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; COMPLEX FORMATION; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY ANALYSIS;

EID: 0842299408     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2003.11.012     Document Type: Article

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28. 5OH (25 mL). The reaction mixture was stirred for 4-6 h at room temperature under argon. The precipitates formed were collected by suction filtration and washed by cold ethanol. The analytically pure product can be obtained when recrystallized from THF/EtOH or purified by flash chromatography on neutral alumina ( n -hexane/ethyl acetate/triethylamine, v/v/v, 80/19/1).
29. 2 : 0.1631. Crystallographic data reported in this paper have been deposited with Cambridge Crystallographic Data center (CCDC No. 208538). Copies of the data can be obtained free of charge from www.ccdc.cam.ac.uk/conts/ retrieving.html (or from the Cambridge Crystallographic Data Center, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam.ac.uk ).