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1
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33748241762
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Willner, I.; Rubin, S. Angew. Chem., Int. Ed. Engl. 1996, 35, 367.
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Angew. Chem., Int. Ed. Engl.
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Willner, I.1
Rubin, S.2
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2
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0028327682
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Hohsaka, T.; Kawashima, K.; Sisido, M. J. Am. Chem. Soc. 1994, 116, 413.
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J. Am. Chem. Soc.
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Hohsaka, T.1
Kawashima, K.2
Sisido, M.3
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3
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0033549733
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(a) Asanuma, H.; Ito, T.; Yoshida, T.; Liang X. G.; Komiyama, M. Angew. Chem., Int. Ed. 1999, 38, 2393-2395.
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Asanuma, H.1
Ito, T.2
Yoshida, T.3
Liang, X.G.4
Komiyama, M.5
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4
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85044700853
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(b) Asanuma, H.; Liang X. G.; Yoshida, T.; Komiyama, M. ChemBioChem. 2000, 2, 39-44.
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ChemBioChem
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Asanuma, H.1
Liang, X.G.2
Yoshida, T.3
Komiyama, M.4
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5
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0034600770
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(c) Yamazawa, A.; Liang, X. G.; Asanuma, H.; Komiyama, M. Angew. Chem., Int. Ed. 2000, 39, 2356-2358.
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Yamazawa, A.1
Liang, X.G.2
Asanuma, H.3
Komiyama, M.4
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6
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0036902245
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(d) Asanuma, H.; Tamaru, D.; Yamazawa, A.; Liu, M. Z.; Komiyama, M. ChemBioChem. 2002, 3, 786-89.
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ChemBioChem
, vol.3
, pp. 786-789
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Asanuma, H.1
Tamaru, D.2
Yamazawa, A.3
Liu, M.Z.4
Komiyama, M.5
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7
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0032481070
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Asanuma, H.; Ito, T.; Komiyama, M. Tetrahedron Lett. 1998, 39, 9015-9018.
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Tetrahedron Lett.
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Asanuma, H.1
Ito, T.2
Komiyama, M.3
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8
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0346843858
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note
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By this combination, X residue is additionally incorporated into the natural full-matched 6-mer duplex.
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9
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0346213278
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note
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Although 1D and 2D NMR spectra of the duplex containing cis-azobenzene were also measured, the spectra were too complicated to be solved because of the thermal instability of the duplex of the cis-form and the influence of the much more stable trans-form duplex (only 70% is isomerized to the cis-form under the conditions employed).
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10
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0347474505
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note
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Proton signals of the pairs of 2 and 6, 3 and 5, 8 and 12, and 9 and 11 on the azobenzene were equivalent to each other even in the duplex.
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11
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0346213279
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note
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All of the NOEs concerning the azobenzene are displayed with lines on the structure in Supporting Information Figure 1.
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12
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0346213283
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note
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Stereoviews of the duplexes from other angles are shown in Supporting Information Figure 2.
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13
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0348104412
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note
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The melting curves of both Azo-α/C and Azo-β/C duplexes either in the trans- or in the cis-form are presented in Supporting Information Figure 3.
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14
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0035898477
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Azobenzene was tethered on the chiral threoninol that has a structure similar to that of the present prochiral 2,2-bis(hydroxymethyl)propionic acid (Asanuma, H.; Takarada, T.; Yoshida, T.; Tamaru, D.; Liang, X.; Komiyama, M. Angew. Chem., Int. Ed. 2001, 40, 2671-2673). A similar dependence in melting temperature (R-form > S-form) for the chirality of the linker was observed. See Supporting Information Scheme. 1 and Supporting Information Table 1.
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(2001)
Angew. Chem. Int. Ed.
, vol.40
, pp. 2671-2673
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Asanuma, H.1
Takarada, T.2
Yoshida, T.3
Tamaru, D.4
Liang, X.5
Komiyama, M.6
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15
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0346843851
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note
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In the present paper, the X residue is additionally incorporated into one strand of the full-matched natural double strands (7-mer/6-mer nonsymmetrical combination). However, placement of a nucleobase as the counterpart of the X residue, such as a 5′-CGAXGTC-3′/3′ -GCTTCAG-5′ (7-mer/7-mer symmetrical combination) duplex, destabilizes the duplex because intercalated trans-azobenzene directly faces the extra nucleobase and a mismatch-like structure is formed.
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16
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0343359244
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Jeener, J.; Meier, B. H.; Bachmann, P.; Ernst, R. R. J. Chem. Phys. 1979, 71, 4546-4553.
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(1979)
J. Chem. Phys.
, vol.71
, pp. 4546-4553
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Jeener, J.1
Meier, B.H.2
Bachmann, P.3
Ernst, R.R.4
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17
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45249127991
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Marion, D.; Ikura, M.; Tschudin, R.; Bax, A. J. Magn. Reson. 1989, 85, 393-399.
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(1989)
J. Magn. Reson.
, vol.85
, pp. 393-399
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Marion, D.1
Ikura, M.2
Tschudin, R.3
Bax, A.4
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19
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0347474503
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note
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2O by use of a 3-9-19 WATER-GATE pulse sequence and confirmed that the sets of restraints for the calculation obtained from Jump and Return and WATERGATE were almost the same.
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20
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0024282849
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Griesinger, C.; Otting, G.; Wüthrich, K.; Freeman, R. J. Am. Chem. Soc, 1988, 110, 7870-7872.
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(1988)
J. Am. Chem. Soc.
, vol.110
, pp. 7870-7872
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Griesinger, C.1
Otting, G.2
Wüthrich, K.3
Freeman, R.4
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22
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0346213277
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note
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This result indicates that spin diffusion at 100 ms is still small and does not affect the distance interpretation. Note that the loose restraints were used for structural calculations.
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24
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0023769808
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Dauber-Osguthorpe, P.; Roberts, V. A.; Osguthorpe, D. J.; Wolff, J.; Genest. M.; Hagler, A. T. Proteins 1988, 4, 31-47.
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(1988)
Proteins
, vol.4
, pp. 31-47
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Dauber-Osguthorpe, P.1
Roberts, V.A.2
Osguthorpe, D.J.3
Wolff, J.4
Genest, M.5
Hagler, A.T.6
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