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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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19
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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20
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For representative examples, see: Mobley, T. A.; Muller, F.; Berger, S. J. Am. Chem. Soc. 1998, 120, 1333. Cabezas, J. A.; Oehlschlager, A. C. J. Am. Chem. Soc. 1997, 119, 3878. Lipshutz, B. H.; Sharma, S.; Ellsworth, E. L. J. Am. Chem. Soc. 1990, 112, 4032. Bertz, S. H. J. Am. Chem. Soc. 1990, 112, 4031. Lipshutz, B. H.; James, B. J. Org. Chem. 1994, 59, 7585. Lipshutz, B. H.; Kozlowski, J. A.; Wilhelm, R. S. J. Org. Chem. 1984, 49, 3943. Bertz, S. H.; Nilsson, K.; Davidson, O.; Snyder, J. P. Angew. Chem., Int. Ed. Engl. 1998, 37, 314.
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Bertz, S.H.1
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Snyder, J.P.4
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(a) Gerold, A.; Jastrzebski, J. T. B. H.; Kronenburg, C. M. P.; Krause, N.; van Koten, G. Angew. Chem., Int. Ed. Engl. 1997, 36, 755.
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31
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0029949483
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For a study on anionic halocuprates, see: Lipshutz, B. H.; Stevens, K. L.; James, B.; Pavlovich, J. G.; Snyder, J. P. J. Am. Chem. Soc. 1996, 118, 6796.
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33
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0013135546
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Taylor, R. J. K., Ed.; Oxford Press: Oxford, U.K.
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(b) Lipshutz, B. H. In Organocopper Reagents: A Practical Approach; Taylor, R. J. K., Ed.; Oxford Press: Oxford, U.K., 1995; pp 105-128.
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Lipshutz, B.H.1
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34
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0346739456
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note
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(a) Available from Aldrich.
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35
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0000796270
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(b) Corey, E. J.; Floyd, D. M.; Lipshutz, B. H. J. Org. Chem. 1978, 43, 3418.
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Corey, E.J.1
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Lipshutz, B.H.3
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36
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0029826917
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(c) Bertz, S. H.; Eriksson, M.; Miao, G.; Snyder, J. P. J. Am. Chem. Soc. 1996, 118, 10906.
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Bertz, S.H.1
Eriksson, M.2
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Snyder, J.P.4
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37
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0346108903
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note
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The optimal flow rate is 20 μL/min on our instrument as per manufacturer specifications.
-
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38
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0346108901
-
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note
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The selected parameters are as follows: sample temperature, -78 °C; source temperature, 25-35 °C; flow rate, 25 uL/min; cone voltage, 20 V; HV lens, 0.75 kV; capillary, 3.75 kV.
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39
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0346739455
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note
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No identifiable copper-containing species were observed in the positive ion ESIMS data on these, or any other, cuprate samples examined.
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41
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0000432178
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Lipshutz, B. H.; Ellsworth, E. L.; Dimock, S. H. J. Am. Chem. Soc. 1990, 112, 5869.
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Lipshutz, B.H.1
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33845553723
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Yamamoto, Y.; Yamamoto, S.; Yatagai, H.; Ishihara, Y.; Maruyama, K. J. Org. Chem. 1982, 47, 119. Yamamoto, Y. Angew. Chem., Int. Ed. Engl. 1986, 25, 947.
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Yamamoto, Y.1
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43
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84985531889
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Yamamoto, Y.; Yamamoto, S.; Yatagai, H.; Ishihara, Y.; Maruyama, K. J. Org. Chem. 1982, 47, 119. Yamamoto, Y. Angew. Chem., Int. Ed. Engl. 1986, 25, 947.
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Yamamoto, Y.1
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44
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85087241940
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note
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2CuLi have thus far not been successful.
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45
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0348000082
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Lipshutz, B. H.; Kozlowski, J. A.; Breneman, C. M. Tetrahedron Lett. 1985, 26, 5911.
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, vol.26
, pp. 5911
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Lipshutz, B.H.1
Kozlowski, J.A.2
Breneman, C.M.3
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46
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0000800084
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See, for example: Alexakis, A.; Mutti, S.; Normant, J. F. J. Am. Chem. Soc. 1991, 113, 6332.
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Alexakis, A.1
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47
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0001040147
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Rossiter, B. E.; Swingle, N. M. Chem. Rev. 1992, 92, 771. Krause, N. Angew. Chem., Int. Ed. Engl. 1998, 37, 283.
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Rossiter, B. E.; Swingle, N. M. Chem. Rev. 1992, 92, 771. Krause, N. Angew. Chem., Int. Ed. Engl. 1998, 37, 283.
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Krause, N.1
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