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Volumn 119, Issue 17, 1997, Pages 3878-3886

Effect of HMPA on the composition of organocyanocuprates. First observation of a 2J(13C-13CN) coupling constant in a vinylcyanocuprate

Author keywords

[No Author keywords available]

Indexed keywords

ACRYLONITRILE; CARBON 13; COPPER DERIVATIVE; CYANIDE; HEMPA; LITHIUM; ORGANIC COMPOUND; TIN;

EID: 0030952109     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja962697n     Document Type: Article
Times cited : (12)

References (32)
  • 26
    • 0009302899 scopus 로고
    • 13C-Labeled acetylenic ether 13 was prepared by the reaction of 1-[(Diethoxyphosphinyl)oxyl]vinyl octyl ether (obtained from reaction of octyl acetate with LDA and diethylchlorophosphate) with t-BuLi according to: Cabezas, J. A.; Oehlschlager, A. C. J. Org. Chem. 1994, 59, 7523.
    • (1994) J. Org. Chem. , vol.59 , pp. 7523
    • Cabezas, J.A.1    Oehlschlager, A.C.2
  • 27
    • 1842281227 scopus 로고    scopus 로고
    • note
    • 1H-NMR spectra at 0°C, was 1.6 kcal/mol.
  • 28
    • 1842276373 scopus 로고
    • Ph.D. Thesis, Simon Fraser University
    • 2 (12). Cabezas, J. A. Ph.D. Thesis, Simon Fraser University, 1994.
    • (1994)
    • Cabezas, J.A.1
  • 30
    • 1842317578 scopus 로고    scopus 로고
    • note
    • 1H-NMR at -78°C by Bertz (ref 16).
  • 31
    • 1842343518 scopus 로고    scopus 로고
    • note
    • The absence of free LiCN in solution, when this cuprate is prepared in THF has been already demostrated by Professor Lipshutz (ref 14).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.