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85030917763
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note
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The enantiomeric purity of the epoxide 5 was estimated to be >99% by chiral GC analysis of the 1-azido-2-trimethylsiloxyheptane derivative using cyclodex-B (30 m × 0.25 mm i.d.) at 50 °C for 1 min, 20 °C/min to 220°C.
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29
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85030914930
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note
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For the measurement of enantiomeric excess, the diol 6 was converted into its dibenzoate. The enantiomeric purity of the dibenzoate was estimated to be 99.5% by chiral HPLC analysis (Chiralcel OD, 98:2 petroleum ether-iPrOH, 1 mL/min, 240 nm).
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0032580376
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(a) . For reviews on ring-closing metathesis, see: Grubbs R.H., Chang S. Tetrahedron. 54:1998;4413-4450 (b) Prunet J. Angew. Chem., Int. Ed. 42:2003;2826-2830.
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Grubbs, R.H.1
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0038373087
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(a) For reviews on ring-closing metathesis, see: Grubbs R.H., Chang S. Tetrahedron. 54:1998;4413-4450 (b) Prunet J. Angew. Chem., Int. Ed. 42:2003;2826-2830.
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Prunet, J.1
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(a) . For reviews on cyclic sulfites/cyclic sulfates, see: Lohray B.B. Synthesis. 1992;1035-1052 (b) Byun H.-S., He L., Bittman R. Tetrahedron. 56:2000;7051-7091.
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Lohray, B.B.1
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(a) . For reviews on cyclic sulfites/cyclic sulfates, see: Lohray B.B. Synthesis. 1992;1035-1052 (b) Byun H.-S., He L., Bittman R. Tetrahedron. 56:2000;7051-7091.
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Byun, H.-S.1
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