NMR Spectroscopy as a Probe of Surfaces of Supported Metal Catalysts

Advances in Catalysis

Volumn 44, Issue C, 1999, Pages 1-117

  Van Der Klink, J J ^a  

^a EPFL   (Switzerland)

Author keywords

(a crystal structure), FID; BCC; body centered cubic; density of states; DOS; electron spin resonance; ESR; EXAFS; extended X ray absorption fine structure; face centered cubic; FCC; Fourier transform; free induction decay; FT; full width at half maximum; FWHM; HCP; hexagonal close packed; highest occupied molecular orbital; HOMO; Infrared or infrared spectroscopy; IR; LDOS; local density of states; lowest unoccupied molecular orbital; LUMO; magic angle spinning; MAS; NMR; nuclear magnetic resonance; polyvinyl pyrrolidone); PVP; Radiofrequency; RF; room temperature; RT; SEDOR; sedor fraction; Sf; SMSI; spin echo double resonance; strong metal support interaction; TEM; TOSS; total suppression of sidebands; transmission electron microscopy

Indexed keywords

EID: 0345990289     PISSN: 03600564     EISSN: None     Source Type: Book Series    
DOI: 10.1016/S0360-0564(08)60512-X     Document Type: Article

References (192)

1. Thomas J.M., and Klinowski J. Adv. Catal. 33 (1985) 199
2. Haw J.F., and Xu T. Adv. Catal. 42 (1998) 115
3. Slichter C.P. Annu. Rev. Phys. Chem. 37 (1986) 25
4. Ansermet J.P., Slichter C.P., and Sinfelt J.H. Prog. NMR Spectrosc. 22 (1990) 401
5. Duncan T.M. Colloids Surf. 45 (1990) 11
6. Pruski M. In: Grant D.M., and Harris R.K. (Eds). "Encyclopedia of Magnetic Resonance" (1996), Wiley, Chichester, UK 4636
7. Derouane E.G., Abdul Hamid S.B., Pasau-Claerbout A., Seivert M., and Ivanova I.I. Stud. Surface Sci. Catalysis 92 (1995) 123
8. Winter J. "Magnetic Resonance in Metals." (1971), Clarendon, Oxford
9. Fukui K., Yonezawa T., and Shingu H. J. Chem. Phys. 20 (1952) 722
10. Hoffmann R. Rev. Mod. Phys. 60 (1988) 601
11. van Santen R. "Theoretical Heterogeneous Catalysis." (1991), World Scientific, Singapore
12. Blyholder G. J. Phys. Chem. 68 (1964) 2772
13. Dundon J.M. J. Chem. Phys. 76 (1982) 2171
14. Curie P. Ann. Chim. Phys. 5 (1895) 289
15. Townes C.H., Herring C., and Knight W.D. Phys. Rev. 77 (1950) 852
16. Dilke M.H., Eley D.D., and Maxted E.B. Nature 161 (1948) 804
17. Seitchik J.A., Gossard A.C., and Jaccarino V. Phys. Rev. 136A (1964) 1119
18. Weisman I.D., and Knight W.D. Phys. Rev. 169 (1968) 373
19. Inoue N., and Sugawara T. J. Phys. Soc. Jpn. 45 (1978) 450
20. Itoh J., and AsayamaKobayashi K. S., Proc. Coll. Ampere 13 (1964) 162
21. Narath A., and Weaver H.T. J. Physique (Paris) 32 (1971) Cl-992
22. Messmer R.P., Knudson S.K., Johnson K.H., Diamond J.B., and Yang C.Y. Phys. Rev. B 13 (1976) 1396
23. Atkins P.W. "Physical Chemistry,"4th (1990), Oxford Univ.Press, Oxford
24. Ponec V., and Bond G.C. "Catalysis by Metals and Alloys." (1995), Elsevier, Amsterdam
25. Kittel C., and Kroemer H. "Thermal Physics." (1980), Freeman, New York
26. Lang N.D. Solid State Phys. 28 (1973) 225
27. Bardeen J. Phys. Rev. 49 (1936) 653
28. Werner C., Schulte F.K., and Bross H. J. Phys. C 8 (1975) 3817
29. Smith J.R., Ying S.G., and Kohn W. Phys. Rev. Lett. 30 (1973) 610
30. Methfessel M., Hennig D., and Scheffler M. Phys. Rev. B 46 (1992) 4816
31. Sung S.-S., and Hoffmann R. J. Am. Chem. Soc. 107 (1985) 578
32. Heine V. Solid State Phys. 35 (1980) 1
33. Friedel J. Adv. Phys. 3 (1954) 446
34. Michaelson H.B. J. Appl. Phys. 48 (1977) 4729
35. Papaconstantopoulos D.A. "Handbook of the Band Structure of Elemental Solids." (1986), Plenum, New York
36. Posternak M., Krakauer K., Freeman A.J., and Koelling D.D. Phys. Rev. B 21 (1980) 5601
37. Mason J. "Multinuclear NMR." (1987), Plenum, New York
38. van der Klink J.J. J. Phys. Condens. Matter 8 (1996) 1845
39. Bucher J.P., and van der Klink J.J. Phys. Rev. B 38 (1988) 11038
40. Clark W.G. Rev. Sci. Instr. 35 (1964) 316
41. Haeberlen U. "High Resolution NMR in Solids: Selective Averaging." (1976), Academic Press, New York
42. Lizak M.J., Gullion T., and Conradi M.S. J. Magnetic Res. 91 (1991) 254
43. Jeener J., Meier B.H., Bachmann P., and Ernst R.R. J. Chem. Phys. 71 (1979) 4546
44. Forséeacute;n S., and Hoffman R.A. J. Chem. Phys. 39 (1963) 2892
45. Chesters M.A., Dolan A., Lennon D., Williamson D.J., and Packer K.J. J. Chem. Soc. Faraday Trans. 86 (1990) 3491
46. Chesters M.A., Packer K.J., Lennon D., and Viner H.E. J. Chem. Soc. Faraday Trans. 91 (1995) 2191
47. Wu X., Gerstein B.C., and King T.S. J. Catal. 118 (1989) 238
48. Uner D.O., Pruski M., and King T.S. J. Catal. 156 (1995) 60
49. Chesters M.A., Packer K.J., Viner H.E., Wright M.A.P., and Lennon D. J Chem. Soc. Faraday Trans. 92 (1996) 4709
50. J Chem. Soc. Faraday Trans. 93 (1997) 2023
51. Chesters M.A., Packer K.J., Viner H.E., and Wright M.A.P. J. Phys. Chem. B 101 (1997) 9995
52. Sanz J., and Rojo J.M. J. Phys. Chem. 89 (1985) 4974
53. Rojo J.M., Belzunegui J.P., Sanz J., and Guil J.M. J. Phys. Chem. 98 (1994) 13631
54. Sheng T.-C., and Gay I.D. J. Catal. 71 (1981) 119
55. Sheng T.-C., and Gay I.D. J. Catal. 71 (1982) 53
56. Rouabah D., Benslama R., and Fraissard J. Chem. Phys. Lett. 179 (1991) 218
57. Hwang S.-J., Uner D.O., King T.S., Pruski M., and Gerstein B.C. J. Phys. Chem. 99 (1995) 3697
58. Chesters M.A., Packer K.J., Viner H.E., Wright M.A.P., and Lennon D. J. Chem. Soc. Faraday Trans. 91 (1995) 2203
59. Buckingham A.D., and Stephens P.J. J. Chem. Soc. (1964) 2747
60. Ruiz-Morales Y., Schreckenbach G., and Ziegler T. Organometallics 15 (1996) 3920
61. Fukai Y. "The Metal-Hydrogen System." (1993), Springer, Berlin
62. Frieske H., and Wicke E. Ber. Bunsenges. Phys. Chem. 77 (1973) 48
63. Gupta M., and Freeman A.J. Phys. Rev. B 17 (1978) 3029
64. Papaconstantopoulos D.A., Klein B.M., Faulkner J.S., and Boyer L.L. Phys. Rev. B 18 (1978) 2784
65. Seymour E.F.W., Cotts R.M., and Williams W.D. Phys. Rev. Lett. 35 (1975) 165
66. Brill P., and Voitläauml;nder J. Ber. Bunsenges. Phys. Chem. 77 (1973) 1097
67. Wicke E., and Nernst G.H. Ber. Bunsenges. Phys. Chem. 68 (1964) 224
68. Barabino D.J., and Dybowski C. Solid State Nucl. Magnetic Resonance 1 (1992) 5
69. Wiley C.L., and Fradin F.Y. Phys. Rev. B 17 (1978) 3462
70. Schoep G.K., Poulis N.J., and Arons R.R. Physica 75 (1974) 297
71. Cornell D.A., and Seymour E.F.W. J. Less-Common Metals 39 (1975) 43
72. Weinert M., and Freeman A.J. Phys. Rev. B 28 (1983) 6262
73. Eastman J.A., Thompson L.J., and Kestel B.J. Phys. Rev. B 48 (1993) 84
74. Stuhr U., Wipf H., Udovic T.J., Weissmueller J., and Gleiter H. J. Phys. Condens. Matter 7 (1995) 219
75. Nandi R.K., Georgopoulos P., Cohen J.B., Butt J.B., Burwell R.L., and Bilderback D.H. J. Catal. 77 (1982) 421
76. Moraweck B., Clugnet G., and Renouprez A. J. Chim. Phys. 83 (1986) 265
77. McCaulley J.A. J. Phys. Chem. 97 (1993) 10372
78. Paul J.-F., and Sautet P. Phys. Rev. B 53 (1996) 8015
79. Wolf R.J., Lee M.W., and Ray J.R. Phys. Rev. Lett. 73 (1994) 557
80. Polisset M., and Fraissard J. Colloids Surf. A 72 (1993) 197
81. Chang T.C., Cheng C.P., and Yeh C.T. J. Chem. Soc. Faraday Trans. 90 (1994) 1157
82. Bond G.C., and Lou H. J. Catal. 147 (1994) 346
83. Candy J.P., Fouilloux P., and Renouprez A.J. J. Chem. Soc. Faraday 176 (1980) 616
84. Frennet A., and Wells P.B. Appl. Catal. 18 (1985) 243
85. Rouabah D., and Fraissard J. Solid State Nucl. Magnetic Resonance 3 (1994) 153
86. Tong Y.Y., and van der Klink J.J. J. Phys. Chem. 98 (1994) 11011
87. K.J. Packer, personal communication
88. de Menorval L.C., and Fraissard J. Chem. Phys. Lett. 77 (1981) 309
89. Chang T.C., Sheng C.P., and Yeh C.T. J. Catal. 138 (1992) 457
90. Rao L.F., Pruski M., and King T.S. J. Phys. Chem. B 101 (1997) 5717
91. Bhatia S., Engelke F., Pruski M., Gerstein B.C., and King T.S. J. Catal. 147 (1994) 455
92. Engelke F., Vincent R., King T.S., and Pruski M. J Chem. Phys. 101 (1994) 7262
93. M. Pruski, personal communication.
94. Engelke F., Bhatia S., King T.S., and Pruski M. Phys. Rev. B 49 (1994) 2730
95. Ito T., and Kadowaki T. Jpn. J. Appl. Phys. 14 (1975) 1673
96. Boudart M., Delbouille A., Derouane E.G., Indovina V., and Walters A.B. J Am. Chem. Soc. 94 (1972) 6622
97. Dennison P.R., Packer K.J., and Spencer M.S. J. Chem. Soc. Faraday Trans. I 85 (1989) 3537
98. Wu X., Gerstein B.C., and King T.S. J. Catal. 121 (1990) 271
99. Smale M.W., and King T.S. J. Catal. 119 (1989) 441
100. Savargaonkar N., Khanra B.C., Pruski M., and King T.S. J. Catal. 162 (1996) 277
101. F. Calderazzo, personal communication
102. Ichikawa S., Poppa H., and Boudart M. J. Catal. 91 (1985) 1
103. Robbins J.L. J. Catal. 115 (1989) 120
104. van't Blik H.F.J., van Zon J.B.A.D., Huizinga T., Vis J.C., Koningsberger D.C., and Prins R. J. Phys. Chem. 87 (1983) 2264
105. Gleeson J.W., and Vaughan R.W. J. Chem. Phys. 78 (1983) 5384
106. Oldfleld E., Keniry M.A., Shinoda S., Schramm S., Brown T.L., and Gutowsky H.S. J. Chem. Soc. Chem. Commun. (1985) 791
107. Wang Z., Ansermet J.-Ph., Slichter C.P., and Sinfelt J.H. J. Chem. Soc. Faraday Trans. I 84 (1988) 3785
108. Compton D.B., and Root T.W. J. Catal. 136 (1992) 199
109. Sharma S.B., Laska T.E., Balaraman P., Root T.W., and Dumesic J.A. J. Catal. 150 (1994) 225
110. der van Putten D., Brom H.B., Witteveen J., de Jongh L.J., and Schmid H. Z. Phys. D 26 (1993) S21
111. Kolbert A.C., de Groot H.J.M., van der Putten D., Brom H.B., de Jongh L.J., Schmid G., Krautscheid H., and Fenske D. Z. Phys. D 26 (1993) S24
112. C.D. Makowka, PhD thesis, University of Illinois, Urbana (1982)
113. S.L. Rudaz, PhD thesis, University of Illinois, Urbana (1984)
114. AnsermetJ.-Ph., PhD thesis, University of Illinois, Urbana (1985)
115. S. Shore, PhD thesis, University of Illinois, Urbana (1986)
116. Z. Wang, PhD thesis, University of Illinois, Urbana (1987)
117. Becerra L.R., Klug C.A., Slichter C.P., and Sinfelt J.H. J. Phys. Chem. 97 (1993) 12014
118. Bradley J.S., Millar J.M., Hill E.W., and Behal S. J. Catal. 129 (1991) 530
119. Zilm K.W., Bonneviot L., Hamilton D.M., Webb G.G., and Haller G.L. J. Phys. Chem. 94 (1990) 1463
120. Rudaz S.L., Ansermet J.-Ph., Wang P.K., Slichter C.P., and Sinfelt J.H. Phys. Rev. Lett. 54 (1985) 71
121. D.J. Durand, PhD thesis, University of Illinois, Urbana (1989)
122. E.J. Dean, PhD thesis, University of Illinois, Urbana (1997)
123. Ansermet J.-Ph., Slichter C.P., and Sinfelt J.H. J. Chem. Phys. 88 (1988) 5963
124. Eischens R.P. Ace. Chem. Res. 5 (1972) 74
125. Shore S.E., Ansermet J.-Ph., Slichter C.P., and Sinfelt J.H. Phys. Rev. Lett. 58 (1987) 953
126. Zilm K.W., Bonneviot L., Haller G.L., Han O.H., and Kermarec M. J. Phys. Chem. 94 (1990) 8495
127. Becerra L.R., Slichter C.P., and Sinfelt J.H. J. Phys. Chem. 97 (1993) 10
128. Becerra L.R., Slichter C.P., and Sinfelt J.H. Phys. Rev. B 52 (1995) 11457
129. Bradley J.S., Millar J.M., Hill E.W., and Melchior M. J. Chem. Soc. Chem. Commun. (1990) 705
130. Bradley J.S., Millar J.M., and Hill E.W. J. Am. Chem. Soc. 113 (1991) 4016
131. Duncan T.M., and Root T.W. J. Phys. Chem. 92 (1988) 4426
132. Duncan T.M., Winslow P., and Bell A.T. Chem. Phys. Lett. 102 (1983) 163
133. Makowka C.D., Slichter C.P., and Sinfelt J.H. Phys. Rev. Lett. 49 (1982) 379
134. Slezak P.J., and Wieckowski A. J. Magnetic Resonance A 102 (1993) 166
135. Wu J., Day J.B., Franaszczuk K., Montez B., Oldfield E., Wieckowski A., Vuissoz P.A., and Ansermet J.-Ph. J. Chem. Soc. Faraday Trans. 93 (1997) 1017
136. Vuissoz P.A., Ansermet J.-Ph., and Wieckowski A. Electrochim. Acta 44 (1998) 1397
137. Day J.B., Vuissoz P.A., Oldfield E., Wieckowski A., and Ansermet J.-Ph. J. Am. Chem. Soc. 118 (1996) 13046
138. Yahnke M.S., Rush B.M., Reimer J.A., and Cairns E.J. J. Am. Chem. Soc. 118 (1996) 12250
139. Wong Y.T., and Hoffmann R. J. Phys. Chem. 95 (1991) 859
140. Hu P., King D.A., Lee M.-H., and Payne M.C. Chem. Phys. Lett. 246 (1995) 73
141. Engel T., and Ertl G. Adv. Catalysis 28 (1979) 1
142. Sheu L.L., Knözinger H., and Sachtler W.M.H. J. Am. Chem. Soc. 111 (1989) 8125
143. Vedrine J.C., and Naccache C. Chem. Phys. Lett. 18 (1973) 190
144. Lunsford J.H., and Jayne J.P. J. Chem. Phys. 44 (1966) 1492
145. P.A. Vuissoz F. Reuse, personal communication
146. Gomer R. Rep. Progr. Phys. 53 (1990) 917 [See Section 4.3.2]
147. Lewis R., and Gomer R. Nuovo Cimento Suppl. 5 (1967) 506
148. Poelsema B., Verheij L.K., and Comsa G. Phys. Rev. Lett. 49 (1982) 1731
149. Seebauer E.G., Kong A.C.R., and Schmidt L.D. J. Chem. Phys. 88 (1988) 6597
150. Kwasniewski V.J., and Schmidt L.D. Surf. Sci. 274 (1992) 329
151. von Oertzen A., Rotermund H.H., and Nettesheim S. Surf. Sci. 311 (1994) 322
152. Froitzheim H., and Schulze M. Surf. Sci. 320 (1994) 85
153. Croci M., Féeacute;lix G., Vandoni G., Harbich W., and Monot R. Surf. Sci. Lett. 290 (1993) L667
154. Wang L., Ge Q., and Billing G.D. Surf. Sci. Lett. 304 (1994) L413
155. Lambert D.K. Electrochim. Acta 41 (1996) 623
156. Persson B.N.J., and Persson M. Solid State Commun. 36 (1980) 175
157. Schmidt M.E., and Guyot-Sionnest P. J. Chem. Phys. 104 (1996) 2438
158. Bucher J.P., Buttet J., van der Klink J.J., and Graetzel M. Surf. Sci. 214 (1989) 347
159. Makowka C.D., Slichter C.P., and Sinfelt J.H. Phys. Rev. B 31 (1985) 5663
160. Tong Y.Y., van der Klink J.J., Clugnet G., Renouprez A.J., Laub D., and Buffat P.A. Surf. Sci. 292 (1993) 276
161. Kleine A., and Ryder P.L. Catal. Today 3 (1988) 103
162. Rhodes H.E., Wang P.-K., Stokes H.T., Slichter C.P., and Sinfelt J.H. Phys. Rev. B 26 (1982) 3559
163. Bucher J.P., Buttet J., van der Klink J.J., Graetzel M., Newton E., and Truong T.B. J. Mol. Catal. 43 (1987) 213
164. Yu I., and Halperin W.P. Phys. Rev. B 47 (1993) 15830
165. King T.S., Goretzke W.J., and Gerstein B.C. J. Catal. 107 (1987) 583
166. Plischke J.K., Benesi A.J., and Vannice M.A. J. Phys. Chem. 96 (1992) 3799
167. Mastikhin V.M., Mudrakovsky I.L., Goncharova S.N., Balzhinimaev B.S., Noskova S.P., and Zaikovsky V.I. React. Kinet. Catal. Lett. 48 (1992) 425
168. Bercier J.J., Jirousek M., Graetzel M., and van der Klink J.J. J. Phys. Condens. Matter 5 (1993) L571
169. Tong Y.Y., and van der Klink J.J. J. Phys. Condens. Matter 7 (1995) 2447
170. Tong Y.Y., Laub D., Schultz-Ekloff G., Renouprez A.J., and van der Klink J.J. Phys. Rev. B 52 (1995) 8407
171. Edwards P.P., and Rao C.N.R. "The Metallic and Nonmetallic States of Matter." (1985), Taylor & Francis, London
172. Luntz A.C., Williams M.D., and Bethune D.S. J. Chem. Phys. 89 (1988) 4381
173. Bucher J.P., van der Klink J.J., and Graetzel M. J. Phys. Chem. 94 (1990) 1209
174. Tong Y.Y., Billy J.J., Renouprez A.J., and van der Klink J.J. J. Am. Chem. Soc. 119 (1997) 3929
175. Tong Y.Y., Méeacute;riaudeau P., Renouprez A.J., and van der Klink J.J. J. Phys. Chem. B 101 (1997) 10155
176. Mannstadt W., and Freeman A.J. Phys. Rev. B 55 (1997) 13298
177. Louie S.G. Phys. Rev. Lett. 42 (1979) 476
178. Feibelman P., and Hamann D.R. Surf. Sci. 149 (1985) 48
179. Tong Y.Y., Martin G.A., and van der Klink J.J. J. Phys. Condens. Matter 6 (1994) L533
180. Ebinger H.D., Jäauml;nsch H.J., Polenz C., Polivka B., Preiss W., Saier V., Veith R., and Fick D. Phys. Rev. Lett. 76 (1996) 656
181. Tong Y.Y., Renouprez A.J., Martin G.A., and van der Klink J.J. Stud. Surface Sci. Catal. 101 (1996) 901
182. Tong Y.Y., Belrose C., Wieckowski A., and Oldfield E. J. Am. Chem. Soc. 119 (1997) 11709
183. Rice C., Tong Y.Y., Oldfield E., and Wieckowski A. Electrochim. Acta 43 (1998) 2825
184. Tong Y.Y., Yonezawa T., Toshima N., and van der Klink J.J. J. Phys. Chem. 100 (1996) 730
185. Ladas S., Dalla Betta R.A., and Boudart M. J. Catal. 53 (1978) 356
186. van Leeuwen D.A., van Ruitenbeek J.M., Schmid G., and de Jongh L.J. Phys. Lett. A 170 (1992) 325
187. Toshima N., Yonezawa T., and Kushihashi K. J. Chem. Soc. Faraday Trans. 89 (1993) 2537
188. Vuissoz P.A., Yonezawa T., Yang D., Kiwi J., and van der Klink J.J. Chem. Phys. Lett. 264 (1997) 366
189. Eichler A., Hafner J., Furthmüuuml;ller J., and Kresse G. Surf. Sci. 346 (1996) 300
190. Chang T.H., Cheng C.P., and Yeh C.T. Mat. Chem. Phys. 22 (1989) 503
191. Kohara T., Yamaguchi M., and Asayama K. J. Phys. Soc. Jpn. 54 (1985) 1537
192. Zhang Z., Suib S.L., Zhang Y.D., Hines W.A., and Budnick J.I. J. Am. Chem. Soc. 110 (1988) 5569