-
1
-
-
20844433475
-
-
(a) S. V. Ley, I. R. Baxendale, R. N. Bream, P. S. Jackson, A. G. Leach, D. A. Longbottom, M. Nesi J. S. Scott, R. I. Storer, and S. J. Taylor, J. Chem. Soc., Perkin Trans. 1, 2000, 3815;
-
(2000)
J. Chem. Soc., Perkin Trans. 1
, pp. 3815
-
-
Ley, S.V.1
Baxendale, I.R.2
Bream, R.N.3
Jackson, P.S.4
Leach, A.G.5
Longbottom, D.A.6
Nesi, M.7
Scott, J.S.8
Storer, R.I.9
Taylor, S.J.10
-
2
-
-
0036534285
-
-
(b) S. V. Ley, I. R. Baxendale, G. Brusotti, M. Caldarelli, A. Massi, and M. Nesi, Il Farmaco, 2002, 57, 321;
-
(2002)
Il Farmaco
, vol.57
, pp. 321
-
-
Ley, S.V.1
Baxendale, I.R.2
Brusotti, G.3
Caldarelli, M.4
Massi, A.5
Nesi, M.6
-
4
-
-
0344582497
-
Supported Reagents, Scavengers in Multi-step Organic Synthesis
-
I. R. Baxendale, R. I. Storer, and S. V. Ley, ed. by M. R. Buchmeiser, VCH Berlin, ISBN 3-527-30630-7
-
(d) Supported Reagents and Scavengers in Multi-step Organic Synthesis, I. R. Baxendale, R. I. Storer, and S. V. Ley in "Polymeric Materials in Organic Synthesis and Catalysis", ed. by M. R. Buchmeiser, VCH Berlin, ISBN 3-527-30630-7, 2003, 53.
-
(2003)
Polymeric Materials in Organic Synthesis and Catalysis
, pp. 53
-
-
-
5
-
-
33746467034
-
-
(a) S. V. Ley, O. Schucht, A. W. Thomas, and P. J. Murray, J. Chem. Soc., Perkin Trans. 1, 1999, 1251;
-
(1999)
J. Chem. Soc., Perkin Trans. 1
, pp. 1251
-
-
Ley, S.V.1
Schucht, O.2
Thomas, A.W.3
Murray, P.J.4
-
6
-
-
33746458894
-
-
(b) J. Habermann, S. V. Ley, and J. S. Scott, J. Chem. Soc., Perkin Trans. 1, 1999, 1253;
-
(1999)
J. Chem. Soc., Perkin Trans. 1
, pp. 1253
-
-
Habermann, J.1
Ley, S.V.2
Scott, J.S.3
-
9
-
-
0037124756
-
-
(e) I. R. Baxendale, S. V. Ley, and C. Puitti, Angew. Chem., Int. Ed., 2002, 41, 2194;
-
(2002)
Angew. Chem., Int. Ed.
, vol.41
, pp. 2194
-
-
Baxendale, I.R.1
Ley, S.V.2
Puitti, C.3
-
10
-
-
0037025957
-
-
(f) I. R. Baxendale, S. V. Ley, M. Nesi, and C. Piutti, Tetrahedron, 2002, 58, 6285;
-
(2002)
Tetrahedron
, vol.58
, pp. 6285
-
-
Baxendale, I.R.1
Ley, S.V.2
Nesi, M.3
Piutti, C.4
-
11
-
-
0036007056
-
-
(g) I. R. Baxendale, G. Brusotti, M. Matsuoka, and S. V. Ley, J. Chem. Soc., Perkin Trans. 1, 2002, 143;
-
(2002)
J. Chem. Soc., Perkin Trans. 1
, pp. 143
-
-
Baxendale, I.R.1
Brusotti, G.2
Matsuoka, M.3
Ley, S.V.4
-
12
-
-
0035982152
-
-
(h) I. R. Baxendale, A. L. Lee, and S. V. Ley, J. Chem. Soc., Perkin Trans 1, 2002, 1850.
-
(2002)
J. Chem. Soc., Perkin Trans. 1
, pp. 1850
-
-
Baxendale, I.R.1
Lee, A.L.2
Ley, S.V.3
-
13
-
-
0037124756
-
-
For other asymmetric synthesis using solid-supported reagents within the group see: (a) I. R. Baxendale, S. V. Ley, and C. Piutti, Angew. Chem., Int. Ed., 2002, 41, 2194;
-
(2002)
Angew. Chem., Int. Ed.
, vol.41
, pp. 2194
-
-
Baxendale, I.R.1
Ley, S.V.2
Piutti, C.3
-
14
-
-
0037025957
-
-
(b) I. R. Baxendale, S. V Ley, C. Piutti, and M. Nesi, Tetrahedron, 2002, 58, 6285;
-
(2002)
Tetrahedron
, vol.58
, pp. 6285
-
-
Baxendale, I.R.1
Ley, S.V.2
Piutti, C.3
Nesi, M.4
-
15
-
-
0036007056
-
-
(c) I. R. Baxendale, G. Brusotti, M. Matsuoka, and S. V. Ley, Chem. Soc., Perkin Trans. 1, 2002, 2, 143.
-
(2002)
Chem. Soc., Perkin Trans. 1
, vol.2
, pp. 143
-
-
Baxendale, I.R.1
Brusotti, G.2
Matsuoka, M.3
Ley, S.V.4
-
16
-
-
0038001604
-
-
(d) R. I. Storer, T. Takemoto, P. S. Jackson, and S. V. Ley, Angew. Chem., Int. Ed., 2003, 42, 2521.
-
(2003)
Angew. Chem., Int. Ed.
, vol.42
, pp. 2521
-
-
Storer, R.I.1
Takemoto, T.2
Jackson, P.S.3
Ley, S.V.4
-
17
-
-
0343263813
-
-
S. M. Kupchan, B. Dasgupta, E. Fujita, and M. L. King, Tetrahedron, 1963, 19, 227.
-
(1963)
Tetrahedron
, vol.19
, pp. 227
-
-
Kupchan, S.M.1
Dasgupta, B.2
Fujita, E.3
King, M.L.4
-
18
-
-
0027472156
-
-
(a) M. L. Martin, M. T. Diaz, M. J. Montero, P. Prieto, and L. San Roman, Planta Med., 1993,59,63;
-
(1993)
Planta Med.
, vol.59
, pp. 63
-
-
Martin, M.L.1
Diaz, M.T.2
Montero, M.J.3
Prieto, P.4
San Roman, L.5
-
19
-
-
0028330137
-
-
(b) A. Morello, I. Lipchenca, B. K. Cassels, H. Speisky, J. Aldunate, and Y. Repetto, Comparative Biochemistry and Physiology Part C: Pharmacology, Toxicology and Endocrinology, 1994, 107, Part 3, 367;
-
(1994)
Comparative Biochemistry and Physiology Part C: Pharmacology, Toxicology and Endocrinology
, vol.107
, Issue.PART 3
, pp. 367
-
-
Morello, A.1
Lipchenca, I.2
Cassels, B.K.3
Speisky, H.4
Aldunate, J.5
Repetto, Y.6
-
20
-
-
0028330137
-
-
(c) A. Morello, I. Lipchenca, B. K. Cassels, H. Speisky, J. Aldunate, and Y. Repetto, Comp. Biochem. Phys. C, 1994, 107, 367;
-
(1994)
Comp. Biochem. Phys. C
, vol.107
, pp. 367
-
-
Morello, A.1
Lipchenca, I.2
Cassels, B.K.3
Speisky, H.4
Aldunate, J.5
Repetto, Y.6
-
21
-
-
0028938214
-
-
(d) B. K. Cassels, M. Asencio, P. Conget, H. Speisky, L.A. Videla, and E. A. Lissi, Pharmacol. Res., 1995, 31, 103;
-
(1995)
Pharmacol. Res.
, vol.31
, pp. 103
-
-
Cassels, B.K.1
Asencio, M.2
Conget, P.3
Speisky, H.4
Videla, L.A.5
Lissi, E.A.6
-
22
-
-
0031010428
-
-
(e) V. R. Hegde, P. Dai, C. Ladislaw, M.G. Patel, M. S. Puar, and J. A. Pachter, Bioorg. Med. Chem. Lett., 1997, 7, 1207;
-
(1997)
Bioorg. Med. Chem. Lett.
, vol.7
, pp. 1207
-
-
Hegde, V.R.1
Dai, P.2
Ladislaw, C.3
Patel, M.G.4
Puar, M.S.5
Pachter, J.A.6
-
23
-
-
0031885777
-
-
(f) M. A. Morales, S. E. Bustamante, G. Brito, D. Paz, and B. K. Cassels, Phythoter. Res., 1998, 12, 103.
-
(1998)
Phythoter. Res.
, vol.12
, pp. 103
-
-
Morales, M.A.1
Bustamante, S.E.2
Brito, G.3
Paz, D.4
Cassels, B.K.5
-
24
-
-
0025848129
-
-
For the first stereoselective synthesis see K. Hashigaki, K. Kan, N. Oais. Y. Takeuchi. and M. Yamato, Chem. Pharm. Bull., 1991, 39, 1126.
-
(1991)
Chem. Pharm. Bull.
, vol.39
, pp. 1126
-
-
Hashigaki, K.1
Kan, K.2
Oais, N.3
Takeuchi, Y.4
Yamato, M.5
-
25
-
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0344582495
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note
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The best results are obtained when the mixture is first heated at 200 °C for 30 min followed by removal under vacuum of the ethanol liberated and heating again at 200 °C for another 30 min. In doing so, one avoids the cleavage of the amide to the starting materials which takes place over prolonged heating at high temperature in the presence of ethanol.
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26
-
-
37049067873
-
-
M.G. Banwell, B. D. Bissett, S. Busato, C. J. Cowden, D. C. R. Hockless, J.W. Holman, R.W. Read, and A. W. Wu, J. Chem. Soc., Chem. Commun., 1995, 2551.
-
(1995)
J. Chem. Soc., Chem. Commun.
, pp. 2551
-
-
Banwell, M.G.1
Bissett, B.D.2
Busato, S.3
Cowden, C.J.4
Hockless, D.C.R.5
Holman, J.W.6
Read, R.W.7
Wu, A.W.8
-
27
-
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85087241235
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note
-
3 in reflux toluene (for experimental conditions see ref. 8 and references therein).
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28
-
-
0029933891
-
-
The asymmetric reduction of the imine has been achieved with good results by Noyori and Baker in solution using ruthenium and rhodium catalysts: (a) N. Uematsu, A. Fujii, S. Hashiguchi, T. Ikariya, and R. Noyori, J. Am. Chem. Soc., 1996, 118, 4916;
-
(1996)
J. Am. Chem. Soc.
, vol.118
, pp. 4916
-
-
Uematsu, N.1
Fujii, A.2
Hashiguchi, S.3
Ikariya, T.4
Noyori, R.5
-
30
-
-
0001705138
-
-
(a) A. J. Bose, F. Greer, and C. C. Price, J. Org. Chem., 1958, 23, 1335;
-
(1958)
J. Org. Chem.
, vol.23
, pp. 1335
-
-
Bose, A.J.1
Greer, F.2
Price, C.C.3
-
31
-
-
0000575009
-
-
(b) K. Yamada, M. Takeda, and T. Iwakuma, Tetrahedron Lett., 1981, 22, 3869;
-
(1981)
Tetrahedron Lett.
, vol.22
, pp. 3869
-
-
Yamada, K.1
Takeda, M.2
Iwakuma, T.3
-
32
-
-
37049097825
-
-
(c) K. Yamada, M. Takeda, and T. Iwakuma, J. Chem. Soc., Perkin Trans. 1, 1983, 265;
-
(1983)
J. Chem. Soc., Perkin Trans. 1
, pp. 265
-
-
Yamada, K.1
Takeda, M.2
Iwakuma, T.3
-
33
-
-
0025852254
-
-
(d) S.Atarashi, H. Tsurumi, T. Fujiwara, and I. Hayakawa, J. Heterocyclic Chem., 1991, 28, 329;
-
(1991)
J. Heterocyclic Chem.
, vol.28
, pp. 329
-
-
Atarashi, S.1
Tsurumi, H.2
Fujiwara, T.3
Hayakawa, I.4
-
36
-
-
37049072775
-
-
H. S. Rzepa, M. L. Webb, A. M. Z. Slawin, and D. J. Williams, J. Chem. Soc., Chemm. Comm., 1991, 765.
-
(1991)
J. Chem. Soc., Chemm. Comm.
, pp. 765
-
-
Rzepa, H.S.1
Webb, M.L.2
Slawin, A.M.Z.3
Williams, D.J.4
-
37
-
-
0342517070
-
-
C. Galeffi, R. La Bua, I. Messana, R. Z. Alcazar, and G. B. M. Bettolo, Gazz. Chim. Ital., 1978, 108, 97.
-
(1978)
Gazz. Chim. Ital.
, vol.108
, pp. 97
-
-
Galeffi, C.1
La Bua, R.2
Messana, I.3
Alcazar, R.Z.4
Bettolo, G.B.M.5
-
39
-
-
0013858578
-
-
(b) T. Kametani, S. Takano, R. Yanase, C. Kibayashi, H. Iida, S. Kano, and K. Sakurai, Chem. Pharm. Bull., 1966, 14, 73.
-
(1966)
Chem. Pharm. Bull.
, vol.14
, pp. 73
-
-
Kametani, T.1
Takano, S.2
Yanase, R.3
Kibayashi, C.4
Iida, H.5
Kano, S.6
Sakurai, K.7
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