Efficient synthesis of 1-(4'-methylbenzoyl)-3,3-diethylthiourea under microwave irradiation using potassium fluoride on alumina

Synthetic Communications

Volumn 30, Issue 6, 2000, Pages 1067-1073

  Marquez H ^a   Plutin A ^a   Rodriguez Y ^a   Perez, E ^a   Loupy, A ^b  

^a UNIVERSITY OF HAVANA   (Cuba)

^b UNIVERSITÉ PARIS SUD   (France)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM OXIDE; POTASSIUM FLUORIDE; THIOUREA DERIVATIVE;

ARTICLE; CATALYST; CHEMICAL REACTION; CHEMICAL STRUCTURE; CONTROLLED STUDY; MICROWAVE IRRADIATION; REACTION ANALYSIS; SYNTHESIS;

EID: 0343674503     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397910008087124     Document Type: Article

References (25)

1. Warshawsky, A.; Fieberg, M.M.B. and Mihalik, P. Sep. Purif. Methods, 1980, 9, 209; Chem. Abst., 1981, 94, 163179v.
2. Warshawsky, A.; Fieberg, M.M.B. and Mihalik, P. Sep. Purif. Methods, 1980, 9, 209; Chem. Abst., 1981, 94, 163179v.
3. Rodríguez, Y. and Macías, A. A study in the alkylation of acylthioureas. Proceedings Symposium of Chemistry Heterocyclic Compounds, 1987, 508.
4. Rodríguez, Y.; Cardeñas, M.C.; Plutín, A.M.; Macías, A. and Del Bosque, J. R. An. Quím., 1995, 91, 696.
5. Ben Alloum, A.; Labiad, B. and Villemin, D. J. Chem. Soc., Chem. Commun., 1989, 607.
6. Gutierrez, E.; Loupy, A.; Bram, G. and Ruiz-Hitzky, E. Tetrahedron Lett., 1989, 30, 945.
7. Varma, R.S.; Varma, M. and Chatterjee, A.K. J. Chem. Soc. Perkin Trans I, 1993, 999.
8. Pérez, E.R.; Marrero, A.L.; Pérez, R. and Autié, M.A. Tetrahedron Lett, 1995, 36, 1779.
9. Caddick, S. Tetrahedron, 1995, 51, 10403.
10. Loupy, A.; Petit, A.; Hamelin, J.; Texier-Boullet, F.; Jacquault, P. and Mathé, D. Synthesis, 1998, 1213.
11. Bram, G.; Loupy, A. and Villemin, D. in "Solid Supports and Catalysts in Organic Synthesis"; Smith K. edit.; Ellis Norwood, PTR Prentice Hall: Chichester, 1992, 302.
12. Vazquez-Tato, M.P. Synlett, 1993, 506.
13. Bosch, A.I.; de la Cruz, P.; Diez-Barra, E.; Loupy, A. and Langa, F. Synlett, 1995, 1259.
14. Oussaid, B.; Berlan, J.; Soufiaoui, M. and Garrigues, B. Synthetic Commun., 1995, 25, 659.
15. Lerestif, J.M.; Bazureau, J.F. and Hamelin, J. Synlett, 1995, 647.
16. Marrero-Terrero, A.L. and Loupy, A., Synlett, 1996, 245.
17. Touaux, B.; Texier-Boullet, F. and Hamelin, J. Heteroatom Chem., 1998, 9, 351.
18. Bose, A.K.; Manhas, M.S.; Banik, B.K. and Robb, E.W. Res. Chem. Intermed, 1994, 20, 1.
19. Villemin, D. and Ricard, M. Tetrahedron Lett., 1984, 25, 1059.
20. Loupy, A. and Tchoubar, B. in "Salt Effects in Organic and Organometallic Chemistry", VCH edit., Weinheim, 1992.
21. Suarez, M.; Loupy, A.; Perez, E.; Moran, L.; Gerona, G.; Morales, A. and Autie, M. Heterocyclic Commun., 1996, 2, 275.
22. Pérez, R.; Pérez, E.; Suárez, M.; Gonzalez, L.; Loupy, A.; Jimeno, M.L. and Ochoa, C. Org. Prep. Proced. Int., 1997, 29 , 671.
23. Limousin, C.; Cléophax, J.; Loupy, A. and Petit, A. Tetrahedron, 1998, 54, 13567.
24. Syassi, B.; Bougrin, K. and Soufiaoui, M. Tetrahedron Lett., 1997, 38, 8855.
25. Clark, J.H. Chem. Rev., 1980, 80, 429.