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0142170260
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10
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0242366999
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note
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int = 0.1355), R(F) = 0.0741 and wR2 = 0.2055 using 10703 reflections with I > 2σ(I).
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11
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0242303956
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note
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Elemental anal. Calcd (found) for 1: C, 39.67 (39.95); H, 4.79 (4.03); N, 14.72 (14.96); F, 7.61 (8.11). Calcd (found) for 2: C, 40.67 (39.83); H, 4.51 (4.12); N, 16.11 (16.58); F, 3.64 (3.84).
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12
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0242335467
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note
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int = 0.0426), R(F) = 0.0849 and wR2 = 0.2400 using 13869 reflections with I > 2σ(I). The data were collected on SRS at CCLRC Daresbury using a Bruker AXS SMART CCD area detector.
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14
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