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and references therein
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12
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0141590702
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note
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2. The crystal structure of 1a shows one pyrazole partially brominated (40%) at the 4-position; similar unexpected chlorination of a pyrazole ligand under mild conditions has been observed elsewhere.
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13
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0034770926
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Pons, J.; Chadghan, A.; Alvarez-Larena, A.; Piniella, J. F.; Ros, J. Inorg. Chem. Commun. 2001, 4, 610.
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Pons, J.1
Chadghan, A.2
Alvarez-Larena, A.3
Piniella, J.F.4
Ros, J.5
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14
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0141479175
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note
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max = 46.56°, 13162 reflections measured (8478 independent, R(int) = 0.0434), R1 = 0.0559 and wR2 = 0.0960 for 3923 reflections with I > 2σ(I) (0.1493 and 0.1192 for all data) and 603 parameters.
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15
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0141590703
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note
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2.
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16
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0141479174
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note
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Modified Varian E4 spectrometer, 9.23 GHz for 1b, 9.10 GHz for 2.
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17
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0141590701
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note
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The discrepancy between g-values determined by EPR or magnetic susceptibility for 1b is attributed to the different nature of those measurements; all populated states contribute to bulk magnetic susceptibility, while fast-relaxing states are not observable by EPR.
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18
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33847802449
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(a) Hay, P. J.; Thibeault, J. C.; Hoffmann, R. J. Am. Chem. Soc. 1975, 97, 4884.
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Hay, P.J.1
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19
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0030901691
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(b) Ruiz, E.; Alemany, P.; Alvarez, S.; Cano, J. J. Am. Chem. Soc. 1997, 119, 1297.
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33847798189
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Crawford, V. H.; Richardson, H. W.; Wasson, J. R.; Hodgson, D. J.; Hatfield, W. E. Inorg. Chem. 1976, 15, 2107.
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21
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0141813832
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note
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3 framework remains invariant in those complexes, the weaker contribution of the μ-pz* ligands is considered constant and ignored in the present discussion.
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22
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0035952126
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x2-y2 ground state are known, i.e.: Gupta, M.; Mathur, P.; Butcher, R. J. Inorg. Chem. 2001, 40, 878.
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Gupta, M.1
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Butcher, R.3
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23
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0141479173
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note
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1′, respectively.
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25
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0001576950
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(b) Hotzelmann, R.; Wieghardt, K.; Flörke, U.; Haupt, H.-J.; Weatherburn, D. C.; Bonvoisin, J.; Blondin, G.; Girerd, J.-J. J. Am. Chem. Soc. 1992, 114, 1681.
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Hotzelmann, R.1
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Bonvoisin, J.6
Blondin, G.7
Girerd, J.-J.8
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