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note
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Typical procedure: A pulverized sample of 4 (0.1 g) was placed in a vial and methylene chloride/cyclohexane (3:7, 1 mL) was added. Upon heating to 50 °C, the mixture turned into a transparent solution. After 24 h at room temperature, a transparent gel formed. A dry gel was obtained by slow evaporation of solvent.
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